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GCMS analysis results, sample AE12478, June 2002

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Laboratory report showing GCMS analysis results for sample AE12478 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014460–000014484

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\052 9 02\124 7 8.D Vial: 20 Acq On : 30 May 2002 1:34 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator), Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak Corr. corr. % of # min scan scan scan TY height area % max. total 1 3.220 21 24 31 PV 5 3195 58708 0.13% 0.025% 2 3.473 62 67 72 PV 4 8370 150926 0.35% 0.064% 3 3.526 72 76 93 W 8 5763 204731 0.47% 0.087% 4 3.720 93 109 130 PV 6 33116 3420974 7.85% 1.448% 5 3.855 130 132 135 W 2 29738 462751 1.06% 0.196%

6 3.884 135 137 142 W 6 27863 680175 1.56% 0.288% 7 3.925 142 144 149 W 5 26755 600153 1.38% 0.254% 8 3.972 149 152 154 W 4 24805 459312 1.05% 0.194% 9 3.996 154 156 158 W 3 23713 297027 0.68% 0.126% 10 4.013 158 159 166 W 6 23155 646147 1.48% 0.273%

11 4.525 240 246 255 W 6 13716 592386 1.36% 0.251% 12 5.012 324 329 335 W 5 9924 257760 0.59% 0.109% 13 5.065 335 338 347 W 6 6271 197453 0.45% 0.084% 14 5.347 383 386 397 W 8 3325 112011 0.26% 0.047% 15 5.947 481 488 511 W 29769 890721 2.04% 0.377% 16 6.904 645 658 PV 5 651 2049 39687 0.09% 0.017% 17 7.122 682 688 699 W 5 3702 97065 0.22% 0.041% 18 8.796 964 973 980 PV 8 2570 63875 0.15% 0.027% 19 9.895 1151 1160 1181 PV 1382641 28279127 64.90% 11.970% 20 12.374 1574 1582 1589 PV 56134 846722 1.94% 0.358% 21 12.492 1595 1602 1606 W 3 2028 40534 0.09% 0.017% 22 12.868 1665 1666 1678 W 5 1791 28895 0.07% 0.012% 23 13.391 1744 1755 1768 PV 2090485 38476185 88.30% 16.286% 24 13.544 1773 1781 1793 W 5593 101132 0.23% 0.043% 25 15.659 2135 2141 2149 W 6 2042 38145 0.09% 0.016%

26 16.699 2313 2318 2322 W 3 2816 52042 0.12% 0.022% 27 17.110 2383 2388 2396 W 4 5170 88307 0.20% 0.037% 28 17.621 2470 2475 2481 W 5 2925 45331 0.10% 0.019% 29 18.526 2617 2629 2644 PV 2211559 42776980 98.17% 18.106% 30 20.107 2892 2898 2904 W 4 2417 45741 0.10% 0.019%

31 20.500 2954 2965 2975 W 1109024 21056524 48.32% 8.913% 32 21.352 3100 3110 3120 W 4 8600 149603 0.34% 0.063% 33 21.717 3167 3172 3179 W 6 1947 34982 0.08% 0.015% 34 22.533 3305 3311 3319 W 2 15311 284747 0.65% 0.121% 35 22.909 3354 3375 3394 PV 2 2121016 43576557 100.00% 18.445% 36 23.062 3394 3401 3410 W 17300 353573 0.81% 0.150% 37 25.048 3731 3739 3749 W 14565 289613 0.66% 0.123% 12478.D 052202.M Mon Jun 03 11:40:19 2002 Page 1

NYC-WTC_000014465

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NYC-WTC_000014465Source: NYC Law Department, mirrored locally

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