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GCMS analysis results, sample AE12478, June 2002

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Laboratory report showing GCMS analysis results for sample AE12478 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014460–000014484

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\052902\12478.D Vial: 20 Acq On : 30 May 2002 1:34 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 03 11:39:47 2002 Quant Results File: 0'52202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon Jun 03 11:32:09 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.90 152 4687732 40.00 ug/L 0.00 10) Napthalene-d8 13.39 136 18899218 40.00 ug/L -0.02 17) Acenapthalene-dlO 18.53 164 10431533 40.00 ug/L -0.01 29) Phenanthranene-dlO 22.91 188 16025364 40.00 ug/L 0.00 37) Chrysene-dl2 30.76 240 9952040 40.00 ug/L -0.05 43) Perylene-dl2 34.66 264 5246157 40.00 ug/L -0.03 System Monitoring Compounds 27) TCMX 20.50 209 2113846 33.60 ug/L -0.01 Spiked Amount 40.000 Recovery 84.00% Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachioroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 13.39 93 -2014 Below Cal # l 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate o.oo 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 149 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 2 8) Azobenzene 20.50 77 34164 N.D. 30) Nnitrosodiphenylamine 20.50 169 41026 0.25 ug/L # 61 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 25.05 149 174087 0.36 ug/L # 96 (#) = qualifier out of range (m) = manual integration 12478.D 052202.M Mon Jun 03 11:40:08 2002 Page 1

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