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GCMS analysis results, sample AE12476, June 2002

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Laboratory report showing GCMS analysis results for sample AE12476 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014406–000014432

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\052902\12476.D Vial: 18 Acq On : 29 May 2002 11:56 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.220 21 24 31 PV 6 4438 62827 0.14% 0.025% 2 3.473 62 67 72 PV 6 6627 132340 0.29% 0.053% 3 3.526 72 76 89 W 4 12587 295834 0.65% 0.118% 4 3.725 94 110 114 PV 6 52667 2597062 5.75% 1.033% 5 3.761 114 116 129 W 8 51812 2529490 5.60% 1.006% 6 3.843 129 130 138 W 6 45042 1377802 3.05% 0.548% 7 3.896 138 139 144 W 3 43153 837397 1.85% 0.333% 8 3.931 144 145 147 W 40364 487960 1.08% 0.194% 9 3.955 147 149 161 W 5 39635 1814500 4.02% 0.722% 10 4.272 201 203 205 W 2 26649 416765 0.92% 0.166% 11 4.295 205 207 218 W 9 24602 991563 2.20% 0.394% 12 4.525 243 246 252 W 5 20715 546564 1.21% 0.217% 13 4.601 257 259 265 W 5 16219 421642 0.93% 0.168% 14 4.854 300 302 308 W 7 9469 247323 0.55% 0.098% 15 5.012 325 329 340 W 7 8565 365974 0.81% 0.146%

16 5.341 381 385 386 W 3 3521 53481 0.12% 0.021% 17 5.594 426 428 437 W 4 2921 74796 0.17% 0.030% 18 5.946 480 488 525 PV 2 35643 1199962 2.66% 0.477% 19 9.578 1103 1106 1110 PV 4 1607 20791 0.05% 0.008% 20 9.660 1110 1120 1128 W 9 1826 53415 0.12% 0.021% 21 9.895 1151 1160 1183 PV 1422722 29362424 65.00% 11.678% 22 10.159 1202 1205 1219 W 6 3312 83442 0.18% 0.033% 23 12.004 1514 1519 1526 W 3 2964 56990 0.13% 0.023% 24 12.374 1574 1582 1596 W 2 43210 686735 1.52% 0.273% 25 12.692 1631 1636 1641 W 3 2108 41119 0.09% 0.016% 26 12.868 1657 1666 1671 W 4 3731 112706 0.25% 0.045% 27 13.156 1708 1715 1723 W 2 3839 81682 0.18% 0.032% 28 13.391 1745 1755 1770 W 2162877 39649983 87.77% 15.769% 29 13.544 1776 1781 1794 W 2 6548 133939 0.30% 0.053% 30 14.219 1891 1896 1903 W 6 1614 29313 0.06% 0.012% 31 15.653 2135 2140 2148 PV 4 1837 37354 0.08% 0.015% 32 15.859 2171 2175 2189 W 5 1575 32851 0.07% 0.013% 33 16.340 2247 2257 2265 W 3 2312 48515 0.11% 0.019% 34 16.705 2313 2319 2322 W 4 3709 66546 0.15% 0.026% 35 16.734 2322 2324 2332 W 5 3363 52672 0.12% 0.021%

36 17.110 2383 2388 2392 W 3 5419 85296 0.19% 0.034% 37 17.621 2460 2475 2486 PV 4 2678 50294 0.11% 0.020%

12476.D 052202.M Mon Jun 03 11:33:42 2002 Page 1

NYC-WTC_000014411

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NYC-WTC_000014411Source: NYC Law Department, mirrored locally

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