GCMS analysis results, sample AE12324, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12324.D Vial: 12 Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Carbonic chloride fluoride Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 4.66 0.37 ug/L 250269 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual / 1 Carbonic chloride fluoride 82 CCIFO 000353-49-1 23/ 2 1,3-Dioxol-2-one 86 C3H203 000872-36-6 9 3 Z,Z-7,11-Hexadecadien-l-ol 238 C16H30O 1000131-01-4 9 4 Acetaldehyde, dimethylhydrazone 86 C4H10N2 007422-90-4 7 Abundance Scan 270 (4.666 min): 12324.D (-268) (-) m/z 47.00 10t.00% "" 47

86 5000 36 58 4.40 4.60 4.80 5.00 0- T-T-p-T 11Pmp00u0——umr m/z 86.00 50.18% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 * Abundance #12296: Carbonic chloride fluoride 47

5000 82 4.40 4.60 4.80 5.00 35 63 m/z 82.00 40.15% 18 0- 1 1 1 . niz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #34604:1,3-Dioxol-2-one 86 29 T^ ,Ii1।i 4.40 4.60 4.80 5.00 42 m/z 36.05; 36.68% 5000 14 58

niz-> 0-TT 20 — 40 60 +71—80 100 120 140 160 180 200 220 240 Abundance #34888: Z,Z-7,11-Hexadecadien-1-ol 86 4.40 4.60 4.80 5.00 m/z 86.90 33.21% 5000 69 41 58

miz-> 0 M 100 20 40 60 80 . 98 113124 140 ■ ■ 1 i ■ ‘ 160172 190 206 223 238 • I 1 । 1 ■ i ' ' 1 1 I 1 1 1 1 I 1 ''' 1 I 1 1 1 1 I 1 1 ' '' 1 1 1 120 140 160 180 200 220 240 4.40 4.60 4.80 5.00

12324.D 052202.M Mon Jun 03 10:52:19 2002 Page 16

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