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GCMS analysis results, sample AE12322, June 2002

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Gas chromatography mass spectrometry results for sample AE12322 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014260–000014280

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document LSC Area percent Report

Data File : C:\MSDCHEM\1\DATA\052902\12322.D Vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.232 22 26 30 PV 5 4440 68220 0.18% 0.031% 2 3.397 53 54 66 PV 3 2565 37282 0.10% 0.017% 3 3.538 74 78 89 W 5 9632 178982 0.46% 0.083% 4 3.696 93 105 126 PV 5 37908 3433148 8.83% 1.583% 5 3.826 126 127 140 W 4 34294 1595979 4.10% 0.736% 6 3.914 140 142 145 W 2 29844 444061 1.14% 0.205% 7 3.937 145 146 161 W 6 30162 1523804 3.92% 0.703% 8 4.031 161 162 166 W 4 25284 493325 1.27% 0.227% 9 4.072 166 169 181 W 9 24275 1201405 3.09% 0.554% 10 4.742 282 283 285 W 2 8552 98705 0.25% 0.046% 11 5.030 326 332 340 W 8 6441 256783 0.66% 0.118% 12 5.283 373 375 379 W 3 3489 50685 0.13% 0.023% 13 5.600 425 429 442 W 3 3009 116316 0.30% 0.054% 14 5.935 476 486 526 PV 367895 7863244 20.21% 3.625% 15 7.715 783 789 801 PV 7 3504 109782 0.28% 0.051%

16 8.790 963 972 976 PV 7 1951 46237 0.12% 0.021% 17 9.278 1052 1055 1065 PV 7 1716 31265 0.08% 0.014% 18 9.895 1150 1160 1177 PV 1290945 25856647 66.47% 11.921% 19 10.165 1201 1206 1216 PV 5 1461 17111 0.04% 0.008% 20 12.004 1514 1519 1525 PV 3 2861 51816 0.13% 0.024% 21 13.391 1744 1755 1774 W 1924672 35166679 90.40% 16.214% 22 13.544 1774 1781 1792 W 5699 123070 0.32% 0.057% 23 13.796 1813 1824 1831 PV 7 1701 41177 0.11% 0.019% 24 14.225 1892 1897 1902 W 5 2134 36322 0.09% 0.017% 25 15.659 2135 2141 2149 W 6 1763 36682 0.09% 0.017% 26 16.123 2212 2220 2227 PV 4 1887 36129 0.09% 0.017% 27 16.705 2309 2319 2331 W 5 3136 69203 0.18% 0.032% 28 17.110 2383 2388 2398 W 4 6435 103971 0.27% 0.048% 29 17.621 2469 2475 2481 PV 3 2980 45436 0.12% 0.021% 30 18.526 2619 2629 2647 W 2053882 38902384 100.00% 17.936% 31 18.779 2660 2672 2680 W 5 2577 45409 0.12% 0.021% 32 20.101 2890 2897 2903 PV 3 3080 51087 0.13% 0.024% 33 20.500 2951 2965 2981 PV 1075910 19887585 51.12% 9.169% 34 21.352 3100 3110 3118 BV 2 8061 122354 0.31% 0.056% 35 22.533 3300 3311 3322 PV 2 14345 258497 0.66% 0.119% 36 22.909 3350 3375 3396 PV 2 1928240 38355252 98.59% 17.684% 37 23.068 3396 3402 3409 W 2 13940 268507 0.69% 0.124% 12322.D 052202.M Mon Jun 03 10:49:27 2002 Page 1

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NYC-WTC_000014265Source: NYC Law Department, mirrored locally

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