GCMS analysis results, sample AE12322, June 2002

NYC 9/11 Public Portal Document Llbrary searcn compound Report Data File : C:\MSDCHEM\1\DATA\052902\12322.D Vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Z,Z-7,11-Hexadecadien-l-ol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.94 2.36 ug/L 1523800 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Z,Z-7,11-Hexadecadien-l-ol 238 C16H30O 1000131-01-4 9 2 Krypton 84 Kr 007439-90-9 A 3 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0/2 4 Acetic acid. dichloro-, ethyl ester 156 C4H6C12O2 000535-15-8 2 Abundance Scan 146 (3,937 min): 12322.D (-145) (-) m/z 84.00 100.00% 47 84

5000 e 36 58 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ • i 1 ' ■ ■ i

3.60 3.80 4.00 4.20 0- ■ ■ i ■ • ■ ■ i ■ ■ ' ■ i • ■ ■ ■ i ■ ■ ■ • i ■ ‘ ■ i ■ • ■ • i 1 ■ ■ ■ i ‘ ‘ m/z 47.10 89.74% miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #34888: Z,Z-7,11-Hexadecadien-1-ol 86

5000 69 ■ ■ i ■ ■ * ' i ' • 1 ‘ i ■ ■ • ‘ i ■ ■ ■ ■ i

41 3.60 3.80 4.00 4.20 58 m/z 49.10 89.38% . 98 113124 140 0- - **dmmm 160 172 190 206 223 238 —mmmamnmmmTr niz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #33829: Krypton 84 rT 1 1 r 3.60 3.80 4.00 4.20 5000 m/z 86.00 85.35%

42 0- 4 ‘ 100 ' 120 ‘ 140 ' 160 ‘ 180 ' 200 220 ‘ 240 niz-> 40 60 80 Abundance . #34862: Imidazol, 4-fluoro- ’ ‘ I ’ ‘ ‘ ’ I 1 ‘ ‘ ‘ I ‘ ‘ ‘ ‘ I 1 • * ‘ I 85 3.60 3.80 4.00 4.20 m/z 84.95 37.73% 5000

59 0 ‘ ‘ i 1 ■ ■ 1 i ' ' ‘ ' i • ■ ■ ■ i ■ ‘ r‘ I 1 1 1 ‘ i ' »• i»•»* i • • • • i • ► j »■ i r ’» ' • । ‘ । ‘ ‘ । ■1 • ■ । * ■ ■ ■ । /z-> 40 60 80 100 120 140 160 180 200 220 240 3.60 3.80 4.00 4.20

12322.D 052202.M Mon Jun 03 10:49:41 2002 Page 8

NYC-WTC_000014272