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GCMS analysis results, sample AE12321, June 2002

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Gas chromatography mass spectrometry results for sample AE12321 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014237–000014259

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\052902\12321.D Vial: 9 Acq On : 29 May 2002 4:36 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.455 62 64 74 PV 5 1983 40581 0.10% 0.017% 2 3.537 74 78 90 W 9 5141 129630 0.31% 0.056% 3 3.714 90 108 110 PV 3 30426 1120072 2.71% 0.480% 4 3.737 110 112 115 W 3 31141 508815 1.23% 0.218% 5 3.761 115 116 129 W 3 29229 1400224 3.39% 0.600%

6 3.843 129 130 136 W 5 27545 700935 1.70% 0.300% 7 3.890 136 138 146 W 7 24848 853898 2.07% 0.366% 8 3.949 146 148 155 W 6 22957 700810 1.70% 0.300% 9 4.007 155 158 171 W 7 22303 1129244 2.74% 0.484% 10 4.184 184 188 194 W 6 18048 597068 1.45% 0.256% 11 5.053 333 336 340 W 5 6071 112677 0.27% 0.048% 12 5.371 385 390 397 W 7 4509 139449 0.34% 0.060% 13 5.929 478 485 505 PV 342489 7261721 17.59% 3.112% 14 6.052 505 506 516 W 7 3596 85403 0.21% 0.037% 15 7.721 785 790 794 PV 6 3638 68729 0.17% 0.029%

16 7.756 794 796 800 W 4 2074 26755 0.06% 0.011% 17 9.895 1152 1160 1181 PV 1363923 27304979 66.13% 11.703% 18 13.391 1744 1755 1773 PV 2032160 36684020 88.85% 15.723% 19 13.549 1776 1782 1789 W 2 5663 92431 0.22% 0.040% 20 15.665 2135 2142 2145 PV 5 1296 22780 0.06% 0.010% 21 16.705 2314 2319 2326 W 2 2998 49523 0.12% 0.021% 22 17.110 2382 2388 2395 W 5 5980 90973 0.22% 0.039% 23 17.621 2469 2475 2481 BV 3 3175 48434 0.12% 0.021% 24 18.526 2617 2629 2651 PV 2152255 40770307 98.75% 17.474% 25 20.101 2890 2897 2904 W 2 2963 50086 0.12% 0.021%

26 20.506 2953 2966 2975 PV 1134313 21187144 51.32% 9.081% 27 21.358 3105 3111 3117 W 2 8558 133909 0.32% 0.057% 28 22.463 3287 3299 3304 W 6 1802 42414 0.10% 0.018% 29 22.533 3304 3311 3320 W 2 15375 279815 0.68% 0.120% 30 22.909 3364 3375 3394 PV 2 2032983 41287807 100.00% 17.696% 31 23.062 3394 3401 3417 W 17171 348792 0.84% 0.149% 32 23.779 3511 3523 3529 PV 2 6089 103849 0.25% 0.045% 33 23.849 3529 3535 3540 W 4 2361 46254 0.11% 0.020% 34 24.049 3557 3569 3574 W 4 3336 64142 0.16% 0.027% 35 24.114 3574 3580 3586 W 4 3787 73465 0.18% 0.031% 36 24.255 3594 3604 3609 W 4 4700 94202 0.23% 0.040% 37 24.337 3612 3618 3628 W 7 2212 59259 0.14% 0.025% 12321.D 052202.M Mon Jun 03 10:48:19 2002 Page 1

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NYC-WTC_000014242Source: NYC Law Department, mirrored locally

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