GCMS analysis results, sample AE12288, June 2002

NYC 9/11 Public Portal Document LSU Area Percent Keport Data File : C:\MSDCHEM\l\DATA\052902\12288.D Vial: 7 Acq On : 29 May 2002 2:58 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integratdr) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.579 83 85 92 PV 5 2864 45658 ' 0.11% 0.020% 2 3.714 92 108 110 W 3 26089 978621 • 2.31% 0.426% 3 3.743 110 113 120 W 5 26537 893623 2.11% 0.389% 4 3.796 120 122 124 W 3 24759 301839 0.71% 0.131% 5 3.814 124 125 132 W 7 24648 669249 1.58% 0.291%

6 3.861 132 133 140 W 5 22676 580596 1.37% 0.253% 7 3.908 140 141 150 W 3 21855 762992 1.80% 0.332% 8 4.225 193 195 202 W 5 15047 443198 1.04% 0.193% 9 4.648 266 267 272 W 4 7955 144099 0.34% 0.063% 10 5.071- 335 339 343 W 5 4653 104814 0.25% 0.046%

11 5.365 383 389 410 W 8 5505 230810 0.54% 0.100% 12 5.935 480 486 513 PV 339147 6913864 16.30% 3.007% 13 6.399 561 565 572 W 5 3093 61597 0.15% 0.027% 14 6.610 589 601 605 W 2 8982 179696 0.42% 0.078% 15 6.646 605 607 625 W 7 6102 149875 0.35% 0.065%

16 6.793 631 632 634 PV 1706 8844 0.02% 0.004% 17 7.139 684 691 703 W 7 3219 80436 0.19% 0.035% 18 7.727 783 791 797 PV 6 2813 67907 0.16% 0.030% 19 9.895 1150 1160 1179 PV 1452489 28594959 67.42% 12.437% 20 10.053 1183 1187 1191 W 5 4391 85658 0.20% 0.037%

21 10.165 1199 1206 1216 W 38782 704444 1.66% 0.306% 22 13.391 1745 1755 1776 PV 2112666 38564819 90.92% 16.773% 23 13.549 1776 1782 1797 W 2 5638 117749 0.28% 0.051% 24 16.705 2312 2319 2325 BV 2822 48591 0.11% 0.021% 25 17.110 2383 2388 2398 W 4 5578 87829 0.21% 0.038%

26 17.627 2454 2476 2479 PV 6 2348 49217 0.12% 0.021% 27 18.526 2619 2629 2641 BV 2257268 42415286 100.00% 18.448% 28 18.608 2641 2643 2649 W 5 2027 40632 0.10% 0.018% 29 20.101 2889 2897 2902 PV 2 2194 33957 0.08% 0.015% 30 20.500 2954 2965 2979 W 1135583 21107995 49.77% 9.181%

31 21.358 3105 3111 3118 W 8106 131682 0.31% 0.057% 32 22.539 3304 3312 3321 W 2 14530 262755 0.62% 0.114% 33 22.909 3363 3375 3390 PV 2 2093454 42083673 99.22% 18.304% 34 23.003 3390 3391 3394 W 2 2006 22754 0.05% 0.010% 35 23.068 3394 3402 3414 W 15467 316041 0.75% 0.137%

36 30.759 4698 4711 4738 PV 2 1257295 27233047 64.21% 11.845% 37 30.929 4738 4740 4754 W 9 4305 108556 0.26% 0.047%

12288.D 052202.M Mon Jun 03 09:36:57 2002 Page 1

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