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GCMS analysis results, sample AE12288, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE12288 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014189–000014213

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document Library searcn compoura keport Data File : C:\MSDCHEM\1\DATA\052902\12288.D Vial: 7 Acq On : 29 May 2002 2:58 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Methylene Chloride Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 4.65 0.20 ug/L 144099 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methylene Chloride 84 CH2C12 000075-09-2 74 2 Methylene Chloride 84 CH2C12 000075-09-2 3 Methylene Chloride 84 CH2C12 000075-09-2 9 4 Methylene Chloride 84 CH2C12 000075-09-2 7 Abundance Scan 267 (4.648 min): 12288.D (-266) (-) m/z 49.10 100.00% 49

86 5000 43 1 ' * * I 1 ’ * 1 1 * * * ' I 1 1 * 1 I * ‘ ‘ 4.40 4.60 4.80 5.00 0 WTIWTLTTTPTmmmmPpm 35 40 I m/z 86.00 53.87% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12327: Methylene Chloride 49 84 5000 4.40 4.60 4.80 5.00

miz-> Abundance 01 14 18 24 2831 353841 11 TUHTTTTTTTTTHNTT ,82................ 70............ . - 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #111040: Methylene Chloride 49 88

y_ m/z 84.00 45.68%

84 4.40 4.60 4.80 5.00

miz-> 5000

Of 14 TTTTTHTTHHr 35 2528 32 ,3841 + +2 70 TITCBummmmmpt ■ ■ i" • 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 88 H Myhta... m/z 51.00 37.48%

Abundance #111039: Methylene Chloride ‘ ‘ ‘ I • ‘ ‘ ‘ l ' ' ■ ' I ■ ‘ ' I ‘ ‘ 49 4.40 4.60 4.80 5.00 m/z 47.00 36.12% 84 5000 "*MAAloW4,. 2831 3538 43 | ,552 57 67 71 77 88 0. ‘11111111 ’TTT 11111111111111111111111111111111 | Fi 11111 ■ 11111 ■ [ 11111111 r| 1111111111 11111 in 1111 /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.40 4.60 4.80 5.00

12288.D 052202.M Mon Jun 03 09:37:07 2002 Page 11

NYC-WTC_000014204

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NYC-WTC_000014204Source: NYC Law Department, mirrored locally

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