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GCMS analysis results for sample AE12474, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.

NYC-WTC_000014102–000014124

Folder label: “GCMS X 5/24/02 A 5/28/02

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Scanned page image, NYC-WTC_000014107
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NYC 9/11 Public Portal Document LSC Area Percent Keporc Data File : C:\MSDCHEM\1\DATA\052802\12474.D Vial: 12 Acq On : 28 May 2002 11:15 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.138 9 10 21 PV 9 2240 65987 1 0.18% 0.032% 2 3.220 21 24 31 PV 8 2869 53346 0.14% 0.026% 3 3.714 92 108 110 PV 3 35315 1328653 3.53% 0.640% 4 3.749 110 114 121 W 8 34493 1277361 3.40% 0.615% 5 3.802 121 123 127 W 4 33493 627752 1.67% 0.302%

6 3.831 127 128 136 W 5 33395 967468 2.57% 0.466% 7 3.884 136 137 146 W 7 29378 991618 2.64% 0.478% 8 3.943 146 147 155 W 7 26647 827719 2.20% 0.399% 9 4.683 271 273 275 W 3 9269 137698 0.37% 0.066% 10 5.053 334 336 344 W 7 6148 161112 0.43% 0.078%

11 5.365 384 389 402 W 9 4599 169595 0.45% 0.082% 12 5.929 480 485 508 W 270041 6198765 16.48% 2.986% 13 6.158 521 524 533 PV 8 2114 35426 0.09% 0.017% 14 7.715 785 789 797 PV 5 2977 61646 0.16% 0.030% 15 8.073 843 850 858 W 6 1933 44879 0.12% 0.022% 16 9.895 1144 1160 1174 PV 1202673 24585995 65.37% 11.845% 17 10.224 1212 1216 1227 W 7 3093 44553 0.12% 0.021% 18 11.828 1478 1489 1499 PV 4 11109 184542 0.49% 0.089% 19 12.368 1575 1581 1589 W 33665 502791 1.34% 0.242% 20 13.391 1743 1755 1769 PV 1863727 33418518 88.86% 16.100% 21 13.544 1776 1781 1787 W 2 4608 77889 0.21% 0.038% 22 15.212 2059 2065 2071 W 5987 96248 0.26% 0.046% 23 15.471 2104 2109 2119 PV 6 1973 44385 0.12% 0.021% 24 16.705 2309 2319 2331 BV 5 3034 55003 0.15% 0.026% 25 17.104 2383 2387 2398 PV 4 5783 88985 0.24% 0.043% 26 17.621 2470 2475 2481 PV 6 2794 36805 0.10% 0.018% 27 18.526 2619 2629 2645 PV 1993275 37099451 98.64% 17.873% 28 20.500 2954 2965 2978 PV 1040251 19492104 51.83% 9.391% 29 21.352 3097 3110 3124 PV 4 7636 133465 0.35% 0.064% 30 21.716 3167 3172 3177 PV 4 2286 38916 0.10% 0.019% 31 22.533 3304 3311 3325 W 4 12571 232931 0.62% 0.112% 32 22.909 3364 3375 3393 PV 2 1854801 37609470 100.00% 18.119% 33 23.062 3393 340.1 3410 W 13726 272730 0.73% 0.131% 34 30.753 4698 4710 4746 PV 2 1136534 25424818 67.60% 12.249% 35 30.976 4746 4748 4755 W 4 2648 65089 0.17% 0.031% 36 31.335 4798 4809 4818 PV 6 1972 38272 0.10% 0.018% 37 34.649 5362 5373 5428 PV 612823 15037732 39.98% 7.245% 12474.D 052202.M Thu May 30 10:42:54 2002 Page 1

NYC-WTC_000014107

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NYC-WTC_000014107Source: NYC Law Department, mirrored locally

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