GCMS calibration table for TCLP extraction method

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\052802\12287.D Vial: 6 Acq On : 28 May 2002 6:22 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.532 75 77 85 PV 7 1931 26417 0.06% 0.011% 2 3.708 92 107 110 PV 3 46569 1720909 4.15% 0.736% 3 3.737 110 112 114 W 2 48289 650388 1.57% 0.278% 4 3.761 114 116 118 W 3 47480 662052 1.60% 0.283% 5 3.778 118 119 127 W 4 46907 1343028 3.24% 0.575% 6 3.831 127 128 131 W 2 42943 687309 1.66% 0.294% 7 3.861 131 133 137 W 5 40835 783313 1.89% 0.335% 8 3.896 137 139 141 W 2 40260 527627 1.27% 0.226% 9 3.914 141 142 145 W 3 38512 527593 1.27% 0.226% 10 4.354 215 217 231 W 8 21563 1097235 2.65% 0.469% 11 4.448 231 233 236 W 4 18572 300964 0.73% 0.129% 12 4.895 304 309 314 W 5 11964 341831 0.82% 0.146% 13 5.147 347 352 365 W 6 6081 266473 0.64% 0.114% 14 5.283 372 375 377 W 4 4853 52190 0.13% 0.022% 15 5.312 377 380 382 W 4 4579 66546 0.16% 0.028% 16 5.359 382 388 397 W 8 6507 241799 0.58% 0.103% 17 5.588 420 427 433 W 8 5936 142720 0.34% 0.061% 18 5.929 479 485 514 PV 367573 7736528 18.66% 3.310% 19 7.715 785 789 798 PV 8 3362 87357 0.21% 0.037% 20 9.895 1146 1160 1188 PV 1341100 27076404 65.29% 11.586% 21 11.828 1482 1489 1498 PV 5 6399 102464 0.25% 0.044% 22 12.374 1575 1582 1590 PV 21609 330240 0.80% 0.141% 23 13.391 1744 1755 1770 PV 2012433 36679324 88.45% 15.694% 24 13.544 1775 1781 1791 W 5206 104572 0.25% 0.045% 25 15.212 2055 2065 2072 PV 4 3979 69787 0.17% 0.030% 26 15.659 2137 2141 2145 PV 5 1822 27471 0.07% 0.012% 27 16.705 2314 2319 2323 PV 3224 51307 0.12% 0.022% 28 17.110 2382 2388 2395 W 3 7634 108531 0.26% 0.046% 29 17.621 2467 2475 2483 PV 5 2690 50548 0.12% 0.022% 30 18.526 2617 2629 2653 W 2168695 40823710 98.44% 17.468% 31 18.773 2662 2671 2686 PV 3 1827 32329 0.08% 0.014% 32 20.506 2953 2966 2975 PV 1191185 22588077 54.47% 9.665% 33 21.352 3104 3110 3118 PV 4 9072 144135 0.35% 0.062% 34 21.717 3168 3172 3175 W 6 1881 27250 0.07% 0.012% 35 22.533 3303 3311 3319 BV 2 14418 268704 0.65% 0.115% 36 22.909 3364 3375 3394 PV 2 2086651 41471258 100.00% 17.745% 37 23.062 3394 3401 3413 W 2 15935 320148 0.77% 0.137% 12287.D 052202.M Thu May 30 10:40:25 2002 Page 1

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