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← Document results/DEP Box 15/GCMS X 5/24/02 A 5/28/02
Document / 29 pages

GCMS calibration table for TCLP extraction method

Machine-extracted title · confidence 90%

GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013968–000013996

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\l\DATA\052802\11603.D Vial: 9 Acq On : 28 May 2002 8:49 pm Operator: McLean Sample : 5/24 ad re-ext Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.250 25 29 35 W 5 4592 68904 ' 0.16% 0.026% 2 3.367 48 49 53 PV 4 2203 23194 0.05% 0.009% 3 3.549 74 80 93 PV 7 10341 206536 0.47% 0.079% 4 3.708 93 107 108 PV 4 51071 1584843 3.58% 0.609% 5 3.726 108 110 114 W 4 51196 1071733 2.42% 0.412% 6 3.761 114 116 118 W 2 50102 622021 1.40% 0.239% 7 3.778 118 119 123 W 4 49266 829138 1.87% 0.319% 8 3.825 123 127 136 W 6 47587 2098060 4.74% 0.807% 9 3.890 136 138 139 W 2 43370 455612 1.03% 0.175% 10 3.908 139 141 169 W 7 42779 3949509 8.92% 1.518% 11 4.084 169 171 180 W 7 35305 1297518 2.93% 0.499% 12 4.748 283 284 290 W 5 16148 329779 0.74% 0.127% 13 4.789 290 291 301 W 8 14127 505577 1.14% 0.194% 14 4.895 307 309 311 W 3 12253 156662 0.35% 0.060% 15 5.118 343 347 363 W 8 9601 516306 1.17% 0.198% 16 5.377 388 391 396 W 6 7439 171682 0.39% 0.066% 17 5.582 424 426 435 W 6 5136 154273 0.35% 0.059% 18 5.682 441 443 445 W 3 3291 31492 0.07% 0.012% 19 5.935 479 486 510 W 438478 9020591 20.36% 3.468% 20 6.211 530 533 538 W 7 2467 42694 0.10% 0.016% 21 6.634 600 605 608 PV 6 1992 39014 0.09% 0.015% 22 6.657 608 609 616 W 5 2528 44772 0.10% 0.017% 23 6.904 647 651 654 PV 5 2045 25965 0.06% 0.010% 24 7.257 709 711 714 PV 3 1794 13379 0.03% 0.005% 25 7.709 783 788 794 PV 6 5005 113750 0.26% 0.044% 26 7.756 794 796 799 W 3 2519 31550 0.07% 0.012% 27 8.778 966 970 972 W 4 2691 29861 0.07% 0.011% 28 8.796 972 973 978 W 3 2547 28975 0.07% 0.011% 29 9.895 1149 1160 1173 PV 1469295 28894510 65.22% 11.109% 30 11.998 1510 1518 1529 PV 6 2699 55366 0.12% 0.021% 31 12.374 1576 1582 1591 W 17418 270178 0.61% 0.104% 32 12.486 1597 1601 1613 W 5 2897 69237 0.16% 0.027% 33 12.686 1630 1635 1642 PV 3 2478 50149 0.11% 0.019% 34 13.391 1744 1755 1767 PV 2158039 39109487 88.28% 15.036% 35 13.467 1767 1768 1772 W 2 1762 21026 0.05% 0.008% 36 13.549 1772 1782 1787 W 3 5155 100185 0.23% 0.039% 37 15.206 2060 2064 2071 W 2 2257 38355 0.09% 0.015% 11603.D 052202.M Thu May 30 10:38:44 2002 Page 1

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