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GCMS calibration table for TCLP extraction method

Machine-extracted title · confidence 90%

GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013968–000013996

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document Tentatively ldentiried Compound (LSC) summary Operator ID: McLean Date Acquired: 28 May 2002 8:49 pm - Data File: C:\MSDCHEM\1\DATA\052802\11603.D Name: 5/24 ad re-ext Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Acetonitrile, die... 3.55 0.3 ug/L 206536 1 9.90 28894500 40.0 Methylene Chloride 3.71 2.2 ug/L 1584840 1' 9.90 28894500 40.0 Methane, chloro- 3.72 1.5 ug/L 1071730 1 9.90 28894500 40.0 1,3-Dioxol-2-one 3.76 0.9 ug/L 622021 1 9.90 28894500 40.0 Ethane, fluoro- 3.78 1.1 ug/L 829138 1 9.90 28894500 40.0 Krypton 3.83 2.9 ug/L 2098060 1 9.90 28894500 40.0 Acetaldehyde, dim... 3.89 0.6 ug/L 455612 1 9.90 28894500 40.0 Thiophene 3.91 5.5 ug/L 3949510 1 9.90 28894500 40.0 Ethenamine, N-met... 4.08 1.8 ug/L 1297520 1 9.90 28894500 40.0 Methylene Chloride 4.75 0.5 ug/L 329779 1 9.90 28894500 40.0 1-Propyne 4.79 0.7 ug/L 505577 1 9.90 28894500 40.0 1,2,3-Butatriene, .. . 4.89 0.2 ug/L 156662 1 9.90 28894500 40.0 2-Butenal, 3-methyl- 5.12 0.7 ug/L 516306 1 9.90 28894500 40.0 Methylene Chloride 5.38 0.2 ug/L 171682 1 9.90 28894500 40.0 2-Pentanone, 4-hy... 5.93 12.5 ug/L 9020590 1 9.90 28894500 40.0 Cyclopentasiloxan... 12.37 0.3 ug/L 270178 2 13.39 39109500 40.0 Phenanthrene, 9-m... 22.54 0.3 ug/L 285119 4 22.91 44301500 40.0 Anthracene-dlO- 23.06 0.3 ug/L 310555 4 22.91 44301500 40.0 Isobenzofuran-1,3... 30.92 0.3 ug/L 235999 5 30.76 33142000 40.0 Isoquinolinium, 2... 34.82 0.4 ug/L 198573 6 34.66 21585900 40.0

11603.D 052202.M Thu May 30 10:38:56 2002 Page 24

NYC-WTC_000013996

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NYC-WTC_000013996Source: NYC Law Department, mirrored locally

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