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← Document results/DEP Box 15/GCMS X 5/23/02 A 5/29/02
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GCMS unknowns report, DEP Box 15, June 2002

Machine-extracted title · confidence 90%

GCMS analysis results for sample AE12170 dated June 3, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013853–000013863

Folder label: “GCMS X 5/23/02 A 5/29/02

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NYC 9/11 Public Portal Document LSC Area Percent Report : Data File : C:\HPCHEM\1\DATA\MAY2902\12170.D Vial: 12 Acq On : 29 May 2002 10:09 pm Operator: Morgan Sample : gc/ms scan 5/23 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P 2** Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) ses Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.050 323 327 339 rBV 433903 1058658 23.24% 4.190% 2 12.062 759 764 783 rBV 1290642 3263100 71.62% 12.916% 3 15.698 1153 1160 1177 rBV 2029320 4428449 97.20% 17.529% 4 18.351 1443 1449 1460 rBV 19965 55705 1.22% 0.220% 5 20.995 1730 1737 1756 rBV 2145822 4556024 100.00% 18.034% 6 23.134 1960 1970 1978 rBV 1077957 2250999 49.41% 8.910% 7 25.429 2213 2220 2231 rBV 2104651 4382072 96.18% 17.345% 8 25.566 2231 2235 2245 rVB 14940 47014 1.03% 0.186% 9 27.412 2431 2436 2441 rBV 26217 50611 1.11% 0.200% 10 33.471 3089 3096 3111 rBV2 1270132 2960123 64.97% 11.717% 11 37.657 3544 3552 3572 rBV 756918 2210746 48.52% 8.751%

Sum of corrected areas: 25263501 12170.D GCMS0528.M Thu May 30 08:43:11 2002

NYC-WTC_000013858

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NYC-WTC_000013858Source: NYC Law Department, mirrored locally

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