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GCMS unknowns report for sample AE12284, June 2002

Machine-extracted title · confidence 100%

Report documenting analysis for unknown compounds and surrogate recovery in sample AE12284.

NYC-WTC_000013762–000013771

Folder label: “GCMS X 5/23/02 A 5/30/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report • • Data File : C:\HPCHEM\1\DATA\MAY2902\12284.D Vial: 24 Acq On : 30 May 2002 9:55 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.044 323 327 340 rBV 480116 1126109 25.70% 4.452% 2 12.065 760 765 784 rBV 1265168 3101313 70.79% 12.260% 3 14.682 1044 1050 1057 rVB 113379 237637 5.42% 0.939% 4 15.692 1154 1160 1179 rBV 2004039 4211190 96.12% 16.648% 5 20.989 1731 1737 1756 rBV 2054779 4349548 99.28% 17.195% 6 23.128 1961 1970 1979 rBV 951256 2050684 46.81% 8.107% 7 25.423 2213 2220 2231 rBV2 2038534 4381104 100.00% 17.320% 8 27.406 2431 2436 2442 rBV 44146 82978 1.89% 0.328% 9 33.474 3090 3097 3114 rBV2 1441548 3283797 74.95% 12.982% 10 37.651 3544 3552 3572 rBV2 845057 2471021 56.40% 9.769%

Sum of corrected areas: 25295381 12284.D GCMS0528.M Thu May 30 11:09:58 2002

NYC-WTC_0000 13767

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NYC-WTC_000013767Source: NYC Law Department, mirrored locally

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