GCMS analysis results for sample AE12162, June 2002

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Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.291 35 36 40 PV 4 2345 15121 0.04% 0.008% 2 3.538 74 78 93 PV 4 4437 85068 0.23% 0.047% 3 3.726 93 110 115 PV 6 31891 1643477 4.50% 0.913% 4 3.767 115 117 120 W 4 29559 585838 1.60% 0.326% 5 3.796 120 122 127 W 5 28697 640428 1.75% 0.356%

6 3.837 127 129 131 W 3 26558 363215 0.99% 0.202% 7 3.861 131 133 141 W 6 25039 836243 2.29% 0.465% 8 3.919 141 143 145 W 2 22648 310265 0.85% 0.172% 9 3.943 145 147 157 W 5 21469 776362 2.13% 0.431% 10 4.231 194 196 199 W 3 8959 135254 0.37% 0.075%

11 4.266 199 202 205 W 5 8482 139810 0.38% 0.078% 12 4.431 228 230 232 W 3 2180 15843 0.04% 0.009% 13 4.924 312 314 317 PV 4 2132 19184 0.05% 0.011% 14 5.359 386 388 393 W 6 2849 59920 0.16% 0.033% 15 5.682 441 443 452 PV 6 1786 23164 0.06% 0.013%

16 5.935 479 486 512 BV 103956 2533509 6.94% 1.408% 17 9.901 1152 1161 1179 PV 1196899 24441663 66.93% 13.583% 18 13.391 1744 1755 1777 PV 1826892 33116281 90.69% 18.404% 19 13.544 1777 1781 1788 W 4654 79411 0.22% 0.044% 20 16.711 2315 2320 2330 VB 4 2381 40042 0.11% 0.022%

21 18.532 2605 2630 2640 PV 1919910 36517094 100.00% 20.294% 22 20.500 2940 2965 2979 PV 410095 7206934 19.74% 4.005% 23 21.358 3104 3111 3114 PV 3 1545 27074 0.07% 0.015% 24 22.539 3304 3312 3319 W 2 11539 221131 0.61% 0.123% 25 22.915 3363 3376 3396 PV 2 1784955 36406000 99.70% 20.232%

26 23.068 3396 3402 3414 W 11060 227936 0.62% 0.127% 27 30.759 4700 4711 4753 PV 2 1029092 21998362 60.24% 12.225% 28 34.655 5365 5374 5401 W 2 476297 11060540 30.29% 6.147% 29 34.819 5401 5402 5425 W 8 5372 231525 0.63% 0.129% 30 35.371 5484 5496 5505 W 6 2269 79799 0.22% 0.044%

31 36.447 5672 5679 5684 W 5 1972 45873 0.13% 0.025% 32 37.710 5884 5894 5904 W 6 2002 60915 0.17% 0.034%

Sum of corrected areas: 179943279

12162.D 052202.M Wed May 29 09:55:07 2002 Page 1

NYC-WTC_000013648

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NYC-WTC_000013648Source: NYC Law Department, mirrored locally

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