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GCMS analysis results for sample AE12162, June 2002

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Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 29 09:45:51 2002 Quant Results File: 052202.RES Quant-Method : C:\MSDCHEM\1\METHODS\0522 02.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 09:44:24 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 3 6) Fluoroanthene 0.00 202 0 N.D. 3 8) Pyrene 0.00 202 0 N.D. 39) Butylbenzylphthalate 0.00 149 0 N.D. 4 0) Benzo(a)anthracene 30.76 228 16590 N.D. 41) Bis(2-ethylhexyl)phthalate 0.00 149 0 N.D. 42) Chrysene 0.00 228 0 N.D. 44) Di-n-octylphthalate 0.00 149 0 N.D. 45) Benzo(b)fluoranthene 0.00 252 0 N.D. 46) Benzo(k)fluoranthene 0.00 252 0 N.D. 47) Benzo(a)pyrene 0.00 252 0 N.D. 48) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 49) Dibenz(a,h)anthracene 0.00 278 0 N.D. 50) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration (+) = signals summed 12162.D 052202.M Wed May 29 09:54:58 2002 Page 2

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NYC-WTC_000013646Source: NYC Law Department, mirrored locally

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