GCMS calibration data for sample AE11931, May 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C: \MSDCHEM\ 1 \DATA\05230211931.D Vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.232 22 26 31 PV 4 4212 60188 0.17% 0.031% 2 3.538 71 78 86 PV 7 8243 166466 0.46% 0.084% 3 3.714 94 108 134 PV 5 47656 5420499 14.93% 2.750% 4 3.872 134 135 158 W 4 39933 3127514 8.62% 1.587% 5 4.025 158 161 163 W 4 33029 544930 1.50% 0.276%

6 4.043 163 164 166 W 2 32575 346405 0.95% 0.176% 7 4.060 166 167 172 W 4 32445 625749 1.72% 0.317% 8 4.102 172 174 180 W 4 30670 810784 2.23% 0.411% 9 4.149 180 182 184 W 3 29235 381618 1.05% 0.194% 10 4.172 184 186 191 W 5 28354 658302 1.81% 0.334%

11 4.260 198 201 209 W 6 26306 887651 2.45% 0.450% 12 5.365 385 389 403 W 9 6009 274748 0.76% 0.139% 13 5.876 473 476 480 PV 6 1952 34646 0.10% 0.018% 14 5.935 480 486 511 W 229252 5333530 14.69% 2.706% 15 6.317 547 551 556 W 7 1873 18264 0.05% 0.009%

16 6.399 561 565 570 PV 6 2376 27206 0.07% 0.014% 17 7.721 786 790 791 PV 4 1923 22881 0.06% 0.012% 18 7.739 791 793 800 W 8 2194 44663 0.12% 0.023% 19 8.790 966 972 980 PV 6 2615 54238 0.15% 0.028% 20 9.901 1152 1161 1181 PV 1179613 24153881 66.55% 12.255%

21 12.374 1578 1582 1588 W 3 1830 34268 0.09% 0.017% 22 12.492 1599 1602 1609 W 3 2287 39069 0.11% 0.020% 23 12.692 1629 1636 1645 W 2 1962 40884 0.11% 0.021% 24 13.391 1743 1755 1776 PV 1803536 32800354 90.37% 16.642% 25 13.544 1776 1781 1789 W 2 4385 79115 0.22% 0.040%

26 15.659 2132 2141 2146 PV 2 1585 26614 0.07% 0.014% 27 16.711 2314 2320 2334 W 2 2793 58868 0.16% 0.030% 28 17.110 2384 2388 2394 W 3 3923 62693 0.17% 0.032% 29 18.532 2617 2630 2643 PV 1916396 36295057 100.00% 18.415% 30 20.101 2891 2897 2907 W 5 1736 40285 0.11% 0.020%

31 20.506 2954 2966 2978 PV 751269 13576309 37.41% 6.888% 32 21.352 3101 3110 3122 PV 4 4148 70868 0.20% 0.036% 33 22.539 3303 3312 3320 W 2 12462 231645 0.64% 0.118% 34 22.915 3365 3376 3396 PV 2 1812957 36285150 99.97% 18.410% 35 23.068 3396 3402 3414 W 11798 236997 0.65% 0.120%

36 30.759 4698 4711 4740 PV 2 943784 20682947 56.99% 10.494% 37 30.941 4740 4742 4752 W 6 2452 50789 0.14% 0.026%

11931.D 052202.M Wed May 29 09:50:51 2002 Page 1

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