GCMS analysis results for sample AE11926, June 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.

NYC-WTC_000013476–000013495

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\052302\11927.D Vial: 7 Acq On : 23 May 2002 2:51 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.226 22 25 30 PV 6 2890 41730 0.11% 0.019% 2 3.490 69 70 75 PV 5 2038 24617 0.06% 0.011% 3 3.749 91 114 117 PV 5 31218 1855305 4.79% 0.864% 4 3.778 117 119 127 W 5 29522 986455 2.55% 0.459% 5 3.837 127 129 146 W 7 27672 1681426 4.34% 0.783%

6 3.949 146 148 166 W 7 23536 1481903 3.83% 0.690% 7 4.072 166 169 172 W 4 20842 405681 1.05% 0.189% 8 4.266 198 202 211 W 8 16944 727980 1.88% 0.339% 9 4.812 291 295 297 W 4 6566 124824 0.32% 0.058% 10 5.365 385 389 398 W 6 4549 144651 0.37% 0.067%

11 5.929 478 485 513 PV 303158 6601648 17.05% 3.073% 12 7.715 780 789 798 PV 6 4127 82715 0.21% 0.039% 13 9.901 1152 1161 1187 PV 1225377 24959110 64.47% 11.619% 14 12.374 1571 1582 1587 BV 3 1689 18715 0.05% 0.009% 15 12.880 1658 1668 1672 PV 7 1754 49432 0.13% 0.023%

16 13.162 1709 1716 1723 W 2 2752 43555 0.11% 0.020% 17 13.391 1745 1755 1772 PV 1854279 33918182 87.61% 15.789% 18 13.544 1772 1781 1790 W 2 5178 106710 0.28% 0.050% 19 13.790 1817 1823 1827 PV 4 4247 58146 0.15% 0.027% 20 15.659 2132 2141 2152 PV 6 1842 50893 0.13% 0.024%

21 16.705 2311 2319 2324 PV 2 2434 37929 0.10% 0.018% 22 17.110 2375 2388 2395 PV 3 5023 75514 0.20% 0.035% 23 17.621 2472 2475 2482 W 4 2140 31600 0.08% 0.015% 24 18.532 2617 2630 2650 PV 1978120 37556546 97.01% 17.483% 25 20.101 2892 2897 2903 PV 4 3395 65177 0.17% 0.030%

26 20.506 2946 2966 2978 PV 921862 17242786 44.54% 8.027% 27 21.358 3100 3111 3118 BV 2 5949 95314 0.25% 0.044% 28 22.539 3305 3312 3321 PV 3 12596 244254 0.63% 0.114% 29 22.915 3356 3376 3394 PV 2 1919231 38714566 100.00% 18.022% 30 23.068 3394 3402 3411 W 2 12814 248336 0.64% 0.116%

31 30.765 4697 4712 4744 W 2 1340959 29026898 74.98% 13.512% 32 30.959 4744 4745 4763 W 7 2622 88112 0.23% 0.041% 33 31.341 4800 4810 4818 PV 5 2064 39839 0.10% 0.019% 34 34.660 5362 5375 5405 BV 2 766361 17964914 46.40% 8.363% 35 34.843 5405 5406 5411 W 4 1893 24062 0.06% 0.011%

11927.D 052202.M Wed May 29 09:48:11 2002 Page 1

NYC-WTC_000013481

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NYC-WTC_000013481Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE11930, June 2002 · Box DEP Box 15

NYC-WTC_000013551

Laboratory report documenting GCMS analysis of sample AE11930 conducted on June 4, 2002.

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