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GCMS analysis results sample AE11926, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.

NYC-WTC_000013454–000013475

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013459
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C: \MSDCHEM\ 1 \DATA\ 052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.244 22 28 35 PV 7 3833 96901 0.23% 0.042% 2 3.355 44 47 52 PV 5 2030 23471 0.05% 0.010% 3 3.543 74 79 93 PV 5 7525 168575 0.39% 0.072% 4 3.714 93 108 114 PV 6 22966 1180441 2.76% 0.507% 5 3.761 114 116 121 W 5 23367 571737 1.34% 0.246% 6 3.802 121 123 128 W 5 21321 475395 1.11% 0.204% 7 3.837 128 129 131 W 2 20382 252175 0.59% 0.108% 8 3.861 131 133 140 W 6 20184 607739 1.42% 0.261% 9 3.920 140 143 156 W 6 19751 994178 2.32% 0.427% 10 4.043 160 164 177 W 9 16341 846301 1.98% 0.364% 11 4.272 200 203 211 W 7 13854 468138 1.09% 0.201% 12 5.365 382 389 407 W 8 5694 271796 0.63% 0.117% 13 5.935 478 486 513 PV 304181 6402855 14.95% 2.753% 14 7.715 786 789 796 PV 6 2912 63441 0.15% 0.027% 15 8.796 966 973 980 W 7 2176 49811 0.12% 0.021% 16 9.901 1152 1161 1178 PV 1406620 28267136 66.02% 12.152% 17 12.369 1576 1581 1588 PV 3 1661 27820 0.06% 0.012% 18 13.397 1745 1756 1773 PV 2085479 38086732 88.95% 16.373% 19 13.544 1773 1781 1788 W 2 5718 107475 0.25% 0.046% 20 15.665 2126 2142 2149 W 6 1800 37647 0.09% 0.016% 21 16.658 2302 2311 2315 W 2 1951 38302 0.09% 0.016% 22 16.711 2315 2320 2327 W 2 3102 61780 0.14% 0.027% 23 17.110 2373 2388 2395 W 3 4767 84175 0.20% 0.036% 24 17.621 2467 2475 2482 PV 3 2154 26115 0.06% 0.011% 25 18.532 2619 2630 2661 PV 2219596 42254093 98.68% 18.165% 26 20.101 2889 2897 2908 PV 5 2726 69080 0.16% 0.030% 27 20.506 2953 2966 2979 W 850444 16249652 37.95% 6.986% 28 21.352 3106 3110 3117 W 3 5325 93384 0.22% 0.040% 29 22.539 3301 3312 3321 W 3 15962 289121 0.68% 0.124% 30 22.915 3363 3376 3396 PV 2 2079180 42818978 100.00% 18.407% 31 23.068 3396 3402 3414 W 14748 287291 0.67% 0.124% 32 29.937 4566 4571 4582 W 2 1679 32304 0.08% 0.014% 33 30.765 4697 4712 4748 PV 2 1405159 31806422 74.28% 13.673% 34 31.347 4804 4811 4817 W 2 1912 32130 0.08% 0.014% 35 34.661 5363 5375 5410 PV 2 836051 19224142 44.90% 8.264%

36 34.878 5410 5412 5418 W 5 3126 68301 0.16% 0.029% 37 35.371 5490 5496 5511 W 5 1968 63996 0.15% 0.028% 11926.D 052202.M Wed May 29 09:47:48 2002 Page 1

NYC-WTC_000013459

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NYC-WTC_000013459Source: NYC Law Department, mirrored locally

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