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GCMS blank analysis results sample AE11926, May 2002

Machine-extracted title · confidence 90%

Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.

NYC-WTC_000013418–000013443

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013425
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\522LB.D Vial: 3 Acq On : 23 May 2002 11:36 am Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Methylene Chloride Concentration Rank. 2 R.T. EstConc Area Relative to ISTD R.T. 3.74 5.08 ug/L 2651250 1,4-Dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methylene Chloride 84 CH2C12 000075-09-2 94 2 Methylene Chloride 84 CH2C12 000075-09-2 91 3 Methylene Chloride 84 CH2C12 000075-09-2 91 4 Methylene Chloride 84 CH2C12 000075-09-2 32 Abundance Scan 113 (3.743 min): 522LB.D (-93) (-) m/z 49.10 100.00%| 49 84

5000

' 1 t ■ • ■ ■ i ■ ■ 1 1 i ' ' 1-11/1/7/11.7 88 3.40 3.60 3.80 4.00 nfe-> 0 "’IEETT01"E$TE1-1’122211"39 + 3538 42 I tumunmyutimyauiqusiry r.upH 1 — 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 84.00 80.08% Abundance #12327: Methylene Chloride 49 84 5000 3.40 3.60 3.80 4.00 m/z 86.00 51.87% 88 / miz-> 14 18 52______ 70____ 24 2831 353841 0 TDTNTTTDOTTTTT Tuummpmmagurrgomunyutt t 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4 Abundance #111041: Methylene Chloride 49

84 3.40 3.60 3.80 4.00 5000 m/z 51.10 / 24.16%

46 2629 41 | $2 59 65 t. 1111111 88 73 7711 i j i 11 1 Ot TmOm)CTmHHtf [ 11 ■. (, 11.. n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111039: Methylene Chloride 40 3.40 3,60 3.80 4.00 m/z 47.00 16.53% 84 _/ 5000-

57 152TJHuumooutgodt 88 2831 3538 43 0 —ICPmogmtmmtughi 67 71 77 t n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 11

522LB.D 052202.M Wed May 29 09:38:39 2002 Page 4

NYC-WTC_000013425

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NYC-WTC_000013425Source: NYC Law Department, mirrored locally

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