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GCMS calibration table data, sample AE10517, May 22, 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.373 48 50 57 PV 6 2335 37031 0.10% 0.017% 2 3.726 90 110 131 PV 4 40580 3998390 10.68% 1.828% 3 3.861 131 133 140 W 6 29260 837793 2.24% 0.383% 4 3.908 140 141 152 W 8 25613 1005132 2.68% 0.460% 5 3.984 152 154 160 W 5 19611 479386 1.28% 0.219% 6 4.031 160 162 184 W 10 16523 1038625 2.77% 0.475% 7 4.184 184 188 197 W 9 7676 221867 0.59% 0.101% 8 4.266 197 202 207 W 5 4646 77008 0.21% 0.035% 9 4.730 280 281 295 PV 8 1951 71193 0.19% 0.033% 10 5.388 384 393 404 PV 9 3404 121040 0.32% 0.055% 11 5.935 480 486 507 PV 294583 6232151 16.64% 2.849% 12 7.116 683 687 693 PV 7 2180 45857 0.12% 0.021% 13 7.715 782 789 793 PV 9 2491 42970 0.11% 0.020% 14 9.219 1039 1045 1050 PV 4 1538 23451 0.06% 0.011% 15 9.901 1152 1161 1183 W 1239019 25000476 66.77% 11.430% 16 12.374 1578 1582 1588 W 3 2005 34366 0.09% 0.016% 17 13.391 1742 1755 1772 PV 1843723 33549189 89.60% 15.338% 18 13.550 1775 1782 1787 W 2 4692 83409 0.22% 0.038% 19 16.705 2309 2319 2328 W 3 3014 63804 0.17% 0.029% 20 17.110 2376 2388 2393 PV 5 4968 93127 0.25% 0.043% 21 17.627 2465 2476 2483 PV 5 2189 37640 0.10% 0.017% 22 18.532 2620 2630 2643 PV 1972958 36946814 98.67% 16.891% 23 18.920 2692 2696 2703 PV 3 1538 22887 0.06% 0.010% .24 20.101 2890 2897 2903 PV 3 4577 82670 0.22% 0.038% 25 20.506 2955 2966 2974 W 945732 17366109 46.38% 7.939% 26 21.358 3105 3111 3121 W 3 6848 112148 0.30% 0.051% 27 22.539 3305 3312 3321 PV 2 13858 260144 0.69% 0.119% 28 22.915 3365 3376 3396 PV 2 1875209 37445004 100.00% 17.119% 29 23.068 3396 3402 3410 W 2 12566 236151 0.63% 0.108% 30 25.048 3732 3739 3753 PV 18185 337788 0.90% 0.154% 31 30.765 4698 4712 4740 W 2 1248781 28106251 75.06% 12.850% 32 30.941 4740 4742 4761 W 6 3813 150896 0.40% 0.069% 33 31.341 4803 4810 4812 W 3 2563 40510 0.11% 0.019% 34 31.999 4911 4922 4933 PV 2 16387 340704 0.91% 0.156% 35 33.203 5109 5127 5136 PV 2 36669 767974 2.05% 0.351% 36 34.326 5302 5318 5332 PV 57368 1308021 3.49% 0.598% 37 34.660 5364 5375 5416 W 2 740964 17947977 47.93% 8.206% 10517.D 052202.M Wed May 22 11:47:57 2002 Page 1

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NYC-WTC_000013288Source: NYC Law Department, mirrored locally

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