GCMS analysis report sample AE09682, May 23, 2002

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GCMS laboratory report for sample AE09682 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013258–000013276

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document LC area Percent Report Data File : C:\MSDCHEM\l\DATA\052102\9682.D Vial: 18 Acq On : 22 May 2002 3:11 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.720 95 109 111 PV 3 20791 778673 1.81% 0.330% 2 3.755 111 115 119 W 6 20167 529047 1.23% 0.224% 3 3.796 119 122 126 W 4 19543 452999 1.05% 0.192% 4 3.831 126 128 142 W 8 17775 930160 2.16% 0.394% 5 3.925 142 144 155 W 8 17204 707593 1.65% 0.300% 6 4.196 188 190 194 W 5 12715 241021 0.56% 0.102% 7 4.278 201 204 216 W 6 16581 601773 1.40% 0.255% 8 4.654 266 268 272 W 4 5252 101962 0.24% 0.043% 9 5.371 386 390 395 W 5 4125 82264 0.19% 0.035% 10 5.935 473 486 514 PV 381576 7622626 17.73% 3.233% 11 7.709 770 788 806 PV 6 3642 121313 0.28% 0.051% 12 9.901 1151 1161 1175 PV 1451762 28210300 65.60% 11.964% 13 12.374 1575 1582 1587 W 3 2074 33058 0.08% 0.014% 14 13.397 1746 1756 1773 BV 2100393 38221444 88.88% 16.210% 15 13.544 1776 1781 1793 W 5363 104104 0.24% 0.044% 16 15.659 2137 2141 2153 PV 6 1879 35134 0.08% 0.015% 17 16.710 2314 2320 2326 W 2 3417 61135 0.14% 0.026% 18 17.110 2382 2388 2393 W 4 6037 103776 0.24% 0.044% 19 17.621 2470 2475 2486 PV 3 2853 46166 0.11% 0.020% 20 18.532 2619 2630 2652 PV 2214444 42473108 98.77% 18.013% 21 20.101 2890 2897 2905 PV 3 5339 96199 0.22% 0.041% 22 20.506 2954 2966 2989 W 1092614 20307632 47.22% 8.613% 23 21.358 3104 3111 3123 PV 2 8641 135516 0.32% 0.057% 24 22.539 3302 3312 3328 W 2 15928 296480 0.69% 0.126% 25 22.915 3364 3376 3396 PV 2 2048476 43002705 100.00% 18.238% 26 23.068 3396 3402 3414 W 2 13833 274635 0.64% 0.116% 27 25.054 3732 3740 3750 PV 41364 733002 1.70% 0.311% 28 30.765 4700 4712 4756 BV 2 1399346 31129662 72.39% 13.202% 29 31.335 4800 4809 4818 W 6 1855 42282 0.10% 0.018% 30 34.660 5364 5375 5400 PV 2 756571 18180412 42.28% 7.710% 31 34.819 5400 5402 5415 W 7 5852 135962 0.32% 0.058%

Sum of corrected areas: 235792144

9682.D 052202.M Wed May 22 11:46:34 2002 Page 1

NYC-WTC_000013263

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NYC-WTC_000013263Source: NYC Law Department, mirrored locally

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