GCMS analysis report sample AE09679, May 23, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\l\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.743 94 113 118 PV 6 39095 2358273 6.32% 1.111% 2 3.784 118 120 122 W 3 36510 535797 1.43% 0.252% 3 3.802 122 123 127 W 3 34818 629762 1.69% 0.297% 4 3.843 127 130 138 W 5 33145 1183886 3.17% 0.558% 5 3.896 138 139 146 W 5 31137 817642 2.19% 0.385% 6 3.943 146 147 149 W 2 29440 322011 0.86% 0.152% 7 3.966 149 151 155 W 4 29202 662283 1.77% 0.312% 8 4.002 155 157 162 W 4 28289 591813 1.58% 0.279% 9 4.043 162 164 166 W 3 26363 405397 1.09% 0.191% 10 4.090 170 172 180 W 8 24357 870992 2.33% 0.410% 11 4.266 198 202 212 W 4 24132 1032008 2.76% 0.486% 12 5.371 385 390 396 W 7 5632 159399 0.43% 0.075% 13 5.582 424 426 432 W 6 3150 60856 0.16% 0.029% 14 5.935 479 486 513 PV 290541 6213809 16.64% 2.928% 15 7.721 785 790 803 W 5 3125 99293 0.27% 0.047% 16 9.219 1040 1045 1051 PV 5 1757 32752 0.09% 0.015% 17 9.901 1149 1161 1182 PV 1241837 25361617 67.92% 11.950% 18 13.391 1745 1755 1770 PV 1873633 33935281 90.88% 15.990% 19 13.549 1773 1782 1790 W 2 4896 94500 0.25% 0.045% 20 15.659 2137 2141 2146 PV 4 1853 28992 0.08% 0.014% 21 16.710 2311 2320 2327 PV 4 2582 50107 0.13% 0.024% 22 17.116 2383 2389 2402 W 5 4984 89238 0.24% 0.042% 23 17.621 2461 2475 2481 PV 5 2638 36608 0.10% 0.017% 24 18.532 2607 2630 2647 W 1958641 37341522 100.00% 17.595% 25 20.101 2889 2897 2905 W 3 5406 90147 0.24% 0.042% 26 20.506 2942 2966 2983 W 960346 17695351 47.39% 8.338% 27 21.358 3103 3111 3127 PV 2 6570 110635 0.30% 0.052% 28 22.539 3305 3312 3321 PV 2 13017 231934 0.62% 0.109% 29 22.915 3365 3376 3395 W 2 1809767 36535100 97.84% 17.215% 30 23.068 3395 3402 3409 W 3 12268 232018 0.62% 0.109% 31 25.054 3728 3740 3760 PV 23417 418901 1.12% 0.197% 32 30.759 4701 4711 4763 PV 2 1236791 26614093 71.27% 12.540% 33 34.325 5311 5318 5325 W 5 2537 49440 0.13% 0.023% 34 34.660 5363 5375 5416 PV 2 723138 16921825 45.32% 7.973% 35 34.919 5416 5419 5421 W 4 2498 40147 0.11% 0.019% 36 35.383 5487 5498 5504 W 6 4085 105118 0.28% 0.050% 37 36.447 5671 5679 5686 W 7 3865 93055 0.25% 0.044%

9679.D 052202.M Wed May 22 11:45:05 2002 Page 1

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