GCMS analysis report sample AE09678, May 23, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report; Data File : C:\MSDCHEM\1\DATA\052102\9678.D Vial: 16 Acq On : 22 May 2002 1:33 am Operator: Mclean Sample : re-extract Inst : 1nstrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.714 93 108 112 PV 3 49115 2071706 5.98% 1.035% 2 3.743 112 113 116 W 3 50584 697583 2.01% 0.348% 3 3.767 116 117 138 W 6 48044 3441412 9.93% 1.719% 4 3.902 138 140 147 W 6 41167 1282524 3.70% 0.641% 5 3.949 147 148 164 W 5 38334 2093705 6.04% 1.046%

6 4.178 185 187 195 W 6 28878 878879 2.54% 0.439% 7 4.254 195 200 212 W 7 27867 1558749 4.50% 0.779% 8 5.048 333 335 339 W 3 7623 108311 0.31% 0.054% 9 5.194 358 360 366 W 5 5517 114167 0.33% 0.057% 10 5.377 385 391 407 W 4 7215 323681 0.93% 0.162%

11 5.929 480 485 503 PV 267402 6199933 17.89% 3.097% 12 6.041 503 504 512 W 6 4567 88118 0.25% 0.044% 13 7.274 707 714 720 PV 7 1673 38965 0.11% 0.019% 14 7.721 781 790 802 W 6 3560 108677 0.31% 0.054% 15 9.901 1152 1161 1185 PV 1092836 23299274 67.21% 11.637%

16 12.380 1574 1583 1587 PV 6 1905 34696 0.10% 0.017% 17 13.391 1743 1755 1777 PV 1711077 31154838 89.88% 15.561% 18 13.544 1777 1781 1793 W 4835 81653 0.24% 0.041% 19 15.665 2134 2142 2148 PV 4 1725 26844 0.08% 0.013% 20 16.705 2315 2319 2326 PV 4 2836 50321 0.15% 0.025%

21 17.110 2379 2388 2395 W 6 4718 85587 0.25% 0.043% 22 17.621 2469 2475 2481 PV 3 1916 30829 0.09% 0.015% 23 18.526 2613 2629 2648 PV 1868097 34664260 100.00% 17.314% 24 20.101 2889 2897 2907 W 3 5038 92120 0.27% 0.046% 25 20.506 2950 2966 2979 PV 884884 16710736 48.21% 8.347%

26 21.358 3106 3111 3119 W 5 6142 100593 0.29% 0.050% 27 22.539 3303 3312 3320 PV 4 12131 227738 0.66% 0.114% 28 22.909 3359 3375 3394 PV 2 1715641 34647332 99.95% 17.306% 29 23.068 3394 3402 3411 W 2 10335 198813 0.57% 0.099% 30 25.054 3732 3740 3750 PV 22927 414844 1.20% 0.207%

31 30.759 4697 4711 4747 PV 2 1124727 24314979 70.14% 12.145% 32 31.335 4803 4809 4816 W 4 2679 40293 0.12% 0.020% 33 32.816 5046 5061 5063 PV 5 1963 66111 0.19% 0.033% 34 32.863 5063 5069 5071 W 7 2605 57402 0.17% 0.029% 35 32.904 5071 5076 5082 W 6 3420 107274 0.31% 0.054%

36 33.197 5119 5126 5133 W 5 2861 60057 0.17% 0.030% 37 34.320 5313 5317 5325 W 4 3602 84148 0.24% 0.042%

9678.D 052202.M Wed May 22 11:43:20 2002 Page 1

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