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GCMS analysis report sample AE09677, May 23, 2002

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GCMS laboratory report for sample AE09677 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013154–000013183

Folder label: “GCMS X 5/21/02 A 5/21/02

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Scanned page image, NYC-WTC_000013160
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\052102\9677.D Vial: 15 Acq On : 22 May 2002 12:44 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.496 66 71 75 PV 7 2636 36644 0.09% 0.014% 2 3.726 94 110 117 PV 4 28727 1679171 3.91% 0.664% 3 3.773 117 118 121 W 3 27208 338884 . 0.79% 0.134% 4 3.796 121 122 138 W 6 26362 1443566 3.36% 0.571% 5 3.896 138 139 143 W 3 23139 438950 1.02% 0.174% 6 3.925 143 144 154 W 7 22392 781566 1.82% 0.309% 7 3.990 154 155 161 W 5 20607 523093 1.22% 0.207% 8 4.196 183 190 194 W 7 17149 624356 1.45% 0.247% 9 4.272 194 203 214 W 5 20222 1062869 2.47% 0.420% 10 4.401 223 225 227 W 3 12993 168723 0.39% 0.067% 11 4.548 249 250 254 W 4 9960 179708 0.42% 0.071% 12 4.918 309 313 316 W 6 5638 114602 0.27% 0.045% 13 5.371 384 390 394 W 4 4931 136050 0.32% 0.054% 14 5.565 418 423 426 PV 5 2359 33585 0.08% 0.013% 15 5.935 481 486 515 PV 330800 6996099 16.29% 2.766% 16 7.715 784 789 799 PV 4 4181 103003 0.24% 0.041% 17 9.225 1041 1046 1051 W 4 1712 30948 0.07% 0.012% . 18 9.278 1051 1055 1068 W 5 2035 39335 0.09% 0.016% 19 9.901 1142 1161 1177 PV 1394810 27982553 65.16% 11.062% 20 11.828 1484 1489 1496 W 3 2070 33446 0.08% 0.013% 21 12.374 1577 1582 1590 W 4 2355 47902 0.11% 0.019% 22 13.391 1746 1755 1768 PV 2070922 37582070 87.51% 14.857% 23 13.544 1773 1781 1787 W 5640 91942 0.21% 0.036% 24 15.659 2137 2141 2166 W 5 2015 41183 0.10% 0.016% 25 16.711 2313 2320 2334 W 2 3579 65845 0.15% 0.026% 26 17.110 2379 2388 2395 PV 3 6332 111624 0.26% 0.044% 27 17.621 2471 2475 2483 W 4 3018 51107 0.12% 0.020% 28 18.532 2619 2630 2653 PV 2170598 42091284 98.01% 16.640% 29 20.107 2884 2898 2904 PV 3 3975 71329 0.17% 0.028% 30 20.506 2953 2966 2981 W 1071432 20128308 46.87% 7.957% 31 21.358 3104 3111 3121 W 4 7754 130494 0.30% 0.052% 32 22.539 3289 3312 3320 W 3 17011 309598 0.72% 0.122% 33 22.915 3364 3376 3395 PV 2 2096738 42946343 100.00% 16.978% 34 23.068 3395 3402 3411 W 2 14746 287110 0.67% 0.114% 35 24.637 3662 3669 3679 PV 3 1963 31353 0.07% 0.012% 36 25.054 3725 3740 3751 BV 30702 549275 1.28% 0.217% 37 26.358 3956 3962 3966 PV 4 1872 28578 0.07% 0.011% 9677.D 052202.M Wed May 22 11:33:58 2002 Page 1

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NYC-WTC_000013160Source: NYC Law Department, mirrored locally

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