GCMS analysis report sample AE09519, May 23, 2002

NYC 9/11 Public Portal Document LbC area Percert Keporc Data File : C:\MSDCHEM\l\DATA\052102\9519.D Vial: 14 Acq On : 21 May 2002 11:55 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.232 24 26 41 W 4 3234 108744 0.30% 0.050% 2 3.543 74 79 82 PV 5 4287 67032 0.19% 0.031% 3 3.573 82 84 87 PV 4 2129 17578 0.05% 0.008% 4 3.749 94 114 160 PV 6 47999 8621738 24.05% 3.972% 5 4.031 160 162 186 W 4 33736 2709672 7.56% 1.248% 6 4.184 186 188 198 W 9 26135 1049986 2.93% 0.484% 7 4.272 198 203 216 W 9 27321 1438349 4.01% 0.663% 8 4.489 238 240 257 W 10 17842 983916 2.74% 0.453% 9 4.760 284 286 296 W 10 10352 411935 1.15% 0.190% 10 5.177 353 357 364 W 7 4662 141350 0.39% 0.065% 11 5.371 382 390 400 W 8 6234 237402 0.66% 0.109% 12 5.935 479 486 508 PV 301772 6536860 18.24% 3.011% 13 6.140 519 521 528 PV 7 1665 16171 0.05% 0.007% 14 7.715 785 789 802 PV 6 4138 101954 0.28% 0.047% 15 9.901 1150 1161 1181 PV 1162431 23851547 66.54% 10.988% 16 11.828 1484 1489 1494 PV 4 3164 47481 0.13% 0.022% 17 13.391 1746 1755 1773 PV 1747209 31913659 89.03% 14.702% 18 13.544 1773 1781 1791 W 2 5157 105151 0.29% 0.048% 19 16.711 2314 2320 2323 PV 2 3286 53733 0.15% 0.025% 20 16.740 2323 2325 2327 W 2 2138 26019 0.07% 0.012% 21 17.110 2383 2388 2394 W 4 5276 79543 0.22% 0.0'37% 22 17.627 2467 2476 2481 W 5 2101 37531 0.10% 0.017% 23 18.526 2613 2629 2650 W 1869971 35426898 98.83% 16.321% 24 20.107 2893 2898 2904 W 3 3740 58012 0.16% 0.027% 25 20.506 2955 2966 2974 W 903707 16970982 47.34% 7.818% 26 21.358 3103 3111 3119 W 5 5468 104247 0.29% 0.048% 27 22.539 3304 3312 3322 BV 2 12837 227818 0.64% 0.105% 28 22.909 3355 3375 3391 PV 2 1786441 35847614 100.00% 16.515% 29 23.068 3396 3402 3410 W 10842 216049 0.60% 0.100% 30 25.054 3731 3740 3765 PV 26130 511592 1.43% 0.236% 31 30.759 4697 4711 4745 PV 2 1351116 29724228 82.92% 13.694% 32 30.965 4745 4746 4754 W 4 1828 32206 0.09% 0.015% 33 31.335 4801 4809 4824 PV 6 4737 84376 0.24% 0.039% 34 34.320 5309 5317 5322 PV 6 2557 61082 0.17% 0.028% 35 34.660 5347 5375 5403 PV 2 830920 18900033 52.72% 8.707% 36 34.831 5403 5404 5414 W 7 3244 59123 0.16% 0.027% 37 35.377 5490 5497 5506 W 5 3565 82006 0.23% 0.038% 9519.D 052202.M Wed May 22 11:32:22 2002 Page 1

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