GCMS analysis report sample AE09517, May 23, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.185 16 .18 20 W 2 2750 19230 0.05% 0.008% 2 3.244 24 28 55 PV 8 3218 162497 0.40% 0.068% 3 3.543 75 79 86 W 7 3595 68669 0.17% 0.029% 4 3.714 92 108 115 PV 5 36503 2006450 4.89% 0.842% 5 3.767 115 117 122 W 5 36698 885003 2.16% 0.371%

6 3.808 122 124 136 W 5 33859 1571533 3.83% 0.660% 7 3.902 136 140 143 W 5 31191 759667 1.85% 0.319% 8 3.931 143 145 150 W 6 29297 666096 1.62% 0.280% 9 3.972 150 152 154 W 3 26972 334427 0.82% 0.140% 10 3.990 154 155 167 W 8 26951 1124683 2.74% 0.472%

11 4.278 201 204 237 W 5 22618 2058433 5.02% 0.864% 12 4.519 244 245 250 W 4 12971 273793 0.67% 0.115% 13 4.695 274 275 285 W 8 9433 309189 0.75% 0.130% 14 5.377 385 391 401 W 5 6556 206225 0.50% 0.087% 15 5.935 481 486 508 PV 316902 6735828 16.43% 2.827%

16 7.715 786 789 800 PV 7 3454 102763 0.25% 0.043% 17 9.901 1152 1161 1180 PV 1363473 27585851 67.30% 11.578% 18 10.247 1209 1220 1229 PV 8 1542 48655 0.12% 0.020% 19 11.828 1473 1489 1496 PV 2 4184 66247 0.16% 0.028% 20 12.004 1512 1519 1523 W 3 1957 30162 0.07% 0.013%

21 12.374 1572 1582 1589 W 4 2461 45633 0.11% 0.019% 22 13.391 1743 1755 1776 PV 2007832 36932954 90.10% 15.501% 23 .13.550 1776 1782 1791 W 5832 106472 0.26% 0.045% 24 15.665 2136 2142 2146 W 5 1705 29608 0.07% 0.012% 25 16.705 2310 2319 2330 PV 4 3237 75384 0.18% 0.032%

26 17.110 2379 2388 2396 W 5 6109 102344 0.25% 0.043% 27 17.621 2465 2475 2480 PV 5 3192 52029 0.13% 0.022% 28 18.532 2618 2630 2645 PV 2174030 40670063 99.22% 17.070% 29 20.101 2891 2897 2906 W 2 3485 65137 0.16% 0.027% 30 20.506 2954 2966 2978 PV 1032299 19183138 46.80% 8.051%

31 21.358 3103 3111 3118 W 4 7594 130305 0.32% 0.055% 32 22.539 3301 3312 3320 PV 2 15092 285624 0.70% 0.120% 33 22.915 3365 3376 3396 PV 2 2009447 40990712 100.00% 17.204% 34 23.068 3396 3402 3414 W 13655 284788 0.69% 0.120% 35 25.054 3733 3740 3759 W 29062 525861 1.28% 0.221%

36 29.202 4433 4446 4455 PV 3 4168 77904 0.19% 0.033% 37 29.937 4566 4571 4581 W 2 2012 47869 0.12% 0.020%

9517.D 052202.M Wed May 22 11:29:12 2002 Page 1

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