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GCMS analysis report sample AE11908, June 4, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.

NYC-WTC_000013014–000013042

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Methylene Chloride Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 4.00 1.21 ug/L 751370 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methylene Chloride 84 CH2C12 000075-09-2(90 2 Methylene Chloride 84 CH2C12 000075-09-283 3 Methylene Chloride 84 CH2C12 000075-09-2 43 4 Methylene Chloride 84 CH2C12 000075-09-2 9 Abundance Scan 156 (3.996 min): 11908.D (-154) (-) m/z 49.10 100.00% 49

5000

84 36 39,9 0!TTp-rTTp-rrTpT-rTjTTTTp-rrTp-rrr^^ 142 HRm4 MH 88 3.60 3.80 4.00 m/z .84.00 4.20 4.40 22.85% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111041: Methylene Chloride 49 84 5000 3.60 3.80 4.00 4.20 4.40 46 m/z 47.10 ,/ • 16.81% 2629 41 | 52 59 65 73 77 88 0! '■I' ■'“I"' ‘I ■' " l ■■ 1 !■ ■ ■ 'I ■■ "| H U|l l Tammumpupt Hhpmpm niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12327: Methylene Chloride 49 84 3.60 3.80 4.00 4.20 4.40 5000 m/z 81.80 12.43%

88 14 —n 01T]—mm——a 24 2831 353841 || 152 18 OOMHHH ________ 70______ . - |Fi 11111111 i i 1111111 pri 11 n 111111 niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111039: Methylene Chloride 49 JU 3.60 3.80 4.00 4.20 4.40 m/z 39.20 11.18% 84 5000

2831 3538 43 88 0 “I00UB——m—mgm—a—um—hmg I,1"52>, pn 57 67 71 77 i ‘1 “ i ■" • i ■ ■ “ i • ■1 t- n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

11908.D 052202.M Tue May 28 12:15:36 2002 Page 11

NYC-WTC_000013029

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NYC-WTC_000013029Source: NYC Law Department, mirrored locally

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