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GCMS sample analysis results, AE11799, June 3, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.

NYC-WTC_000012794–000012822

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C: \MSDCHEM\1\DATA\052202\11799 .D Vial: 6 Acq On : 22 May 2002 5:54 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator).. Title : 508 Modified GC/MS scan

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.702 94 106 108 PV 3 29325 831340 1.74% 0.302% 2 3.725 108 110 112 W 29869 437982 0.92% 0.159% 3 3.749 112 114 119 W 3 30292 745696 1.56% 0.271% 4 3.796 119 122 125 W 5 28589 573195 1.20% 0.208% 5 3.825 125 127 133 W 6 26969 663811 1.39% 0.241%

6 3.866 133 134 141 W 5 25486 708196 1.48% 0.257% 7 3.919 141 143 149 W 5 23514 593612 1.24% 0.216% 8 4.284 199 205 211 W 2 23987 789911 1.65% 0.287% 9 4.589 255 257 263 W 5 8917 219755 0.46% 0.080% 10 5.036 323 333 342 W 5 5671 268146 0.56% 0.097%

11 5.371 386 390 402 W 8 3939 151750 0.32% 0.055% 12 5.941 481 487 519 PV 470037 9143999 19.15% 3.323% 13 7.133 681 690 699 W 9 3644 78439 0.16% 0.029% 14 7.709 780 788 804 PV 5 5669 175875 0.37% 0.064% 15 8.708 955 958 960 PV 3 1649 15631 0.03% 0.006%

16 9.219 1040 1045 1052 PV 5 2210 38753 0.08% 0.014% 17 9.901 1152 1161 1177 PV 1605747 31945989 66.92% 11.608% 18 11.834 1478 1490 1495 W 5 1714 36269 0.08% 0.013% 19 12.374 1575 1582 1591 PV 148583 2232876 4.68% 0.811% 20 13.397 1746 1756 1774 PV 2290837 42637205 89.32% 15.493%

21 13.549 1774 1782 1790 W 2 6492 121592 0.25% 0.044% 22 15.665 2133 2142 2155 W 3 1954 50155 0.11% 0.018% 23 16.710 2315 2320 2332 PV 3 3446 66171 0.14% 0.024% 24 17.110 2374 2388 2397 W 3 7929 129340 0.27% 0.047% 25 17.621 2469 2475 2487 PV 5 3512 69697 0.15% 0.025%

26 18.532 2618 2630 2647 W 2458335 47106552 98.68% 17.117% 27 18.931 2691 2698 2701 PV 3 1296 21248 0.04% 0.008% 28 20.107 2887 2898 2904 W 4 2030 48215 0.10% 0.018% 29 20.512 2954 2967 2975 W 1264141 24449003 51.22% 8.884% 30 21.358 3105 3111 3118 W 2 10400 177171 0.37% 0.064%

31 21.716 3163 3172 3187 W 4 2546 58764 0.12% 0.021% 32 22.539 3304 3312 3321 W 2 18514 343483 0.72% 0.125% 33 22.915 3364 3376 3395 PV 2 2315652 47736982 100.00% 17.346% 34 23.068 3395 3402 3419 W 16054 313681 0.66% 0.114% 35 29.942 4565 4572 4580 PV 3 2052 . 45881 0.10% 0.017%

36 30.765 4697 4712 4747 PV 2 1589640 35283400 73.91% 12.821% 37 31.341 4804 4810 4818 PV 4 3412 61474 0.13% 0.022%

11799.D 052202.M Tue May 28 12:02:42 2002 Page 1

NYC-WTC_000012799

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NYC-WTC_000012799Source: NYC Law Department, mirrored locally

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