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GCMS blank analysis results, sample AE11799, May 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.

NYC-WTC_000012751–000012778

Folder label: “GCMS X 5-21-02 A 5-22-02

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Scanned page image, NYC-WTC_000012755
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C: \MSDCHEM\ 1 \ DATA\ 052202\521LB.D Vial: 3 Acq On : 22 May 2002 3:27 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.702 95 106 108 PV 2 26231 710558 1.92% 0.341% 2 3.732 108 ill 113 W 4 26522 494472 1.34% 0.237% 3 3.755 113 115 131 W 9 26125 1545091 4.18% 0.741% 4 3.861 131 133 136 W 4 23411 388040 1.05% 0.186% 5 3.884 136 137 142 W 5 22040 445502 1.21% 0.214% 6 3.920 142 143 148 W 4 20549 407455 1.10% 0.195% 7 3.955 148 149 156 W 6 20655 556932 1.51% 0.267% 8 4.266 196 202 212 W 4 20339 829441 2.24% 0.398% 9 4.437 229 231 238 W 5 10298 280925 0.76% 0.135% 10 5.371 385 390 408 W 6 4288 164171 0.44% 0.079% 11 5.929 479 485 515 PV 291717 6466929 17.49% 3.101% 12 7.715 783 789 793 PV 5 3402 65211 0.18% 0.031% 13 7.750 793 795 798 W 2 2341 29210 0.08% 0.014% 14 9.895 1149 1160 1186 PV 1215451 24873709 67.28% 11.928% 15 12.375 1574 1582 1592 W 75470 1146135 3.10% 0.550% 16 13.391 1744 1755 1773 PV 1828801 33256132 89.95% 15.948% 17 13.544 1773 1781 1791 W 5211 103390 0.28% 0.050% 18 16.711 2312 2320 2325 PV 2 2975 48356 0.13% 0.023% 19 17.110 2383 2388 2396 W 3 4674 73957 0.20% 0.035% 20 17.621 2470 2475 2481 PV 4 2203 34511 0.09% 0.017% 21 18.532 2618 2630 2640 PV 1948375 36636523 99.10% 17.569% 22 20.107 2893 2898 2904 PV 3 1868 30573 0.08% 0.015% 23 20.506 2950 2966 2985 PV 968515 18122048 49.02% 8.690% 24 21.358 3105 3111 3122 PV 3 6857 108364 0.29% 0.052% 25 22.539 3305 3312 3326 W 4 12545 235730 0.64% 0.113% 26 22.915 3364 3376 3396 PV 2 1848562 36969813 100.00% 17.728% 27 23.068 3396 3402 3411 W 2 8498 160668 0.43% 0.077% 28 30.759 4700 4711 4747 PV 2 1230645 26336617 71.24% 12.629% 29 33.203 5103 5127 5134 W 4 3304 75256 0.20% 0.036% 30 34.326 5310 5318 5325 PV 2 5335 103203 0.28% 0.049% 31 34.655 5360 5374 5398 PV 2 744832 15981318 43.23% 7.664% 32 34.807 5398 5400 5406 W 7 6896 176182 0.48% 0.084% 33 34.854 5406 5408 5416 W 5 7397 226501 0.61% 0.109% 34 34.943 5416 5423 5425 W 7 7414 199921 0.54% 0.096% 35 34.978 5425 5429 5430 W 4 8101 136207 0.37% 0.065% 36 34.996 5430 5432 5435 W 4 10104 169471 0.46% 0.081% 37 35.025 5435 5437 5444 W 8 8430 233266 0.63% 0.112%

521LB.D 052202.M Tue May 28 11:57:55 2002 Page 1

NYC-WTC_000012755

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NYC-WTC_000012755Source: NYC Law Department, mirrored locally

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