GCMS sample analysis results, AE11575, May 30, 2002

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Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\MAY2 10211575.D Vial: 8 Acq On : 22 May 2002 8:18 am Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.12 18.90 ug/1 1021110 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 Acetoner 58 C3H60 000067-64-1 9 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 4 Propanenitrile, 3-ethoxy- 99 C5H9NO 002141-62-0 7 Abundance Scan 335 (8.115 min): 11575.D (-) m/z 43.05 100.00% 43

5000 59 ... g . 1 . , , , I

miz—> 0 1 " 11" '11' “ '' ‘I '^11' ll....Chilli 69 83 TrTTTp-rTTjTTTTp-rrr^^ 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 i 047 7.80 8.00 8.20 m/z 59.10 8.40 37.47% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ■ ■ ■ i ■ ■ ■ ' i • ■ ■ ■ i ■~ ' i ■ • • ■ i 59 7.80 8.00 8.20 8.40 m/z 58.10 17.69% 27 101

miz—> mHTm . 49 tmnunmH 83 i ■ ■'11' ‘ ■ ■ । ■' ■ ■ । ■" ■ । ■ ■1 ■ i ■ ■ ‘ ■ । 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 11ii 111.1111111 J.।

Abundance #62322: Acetone 43 - 7.80 8.00 8.20 8.40 5000 m/z 101.15 11.75% 58 27 ' ‘"'i '■" 111 'h'" ‘i" Ji|l • j > ■' 11 ■ * ’1 j ■ • ' i"»• t > *'' i * • > * i “ ■' J1 ‘4 *: * “ ■ i * • • • j ■ ■ • > i ‘* i “'' j ■1 miz—> 15 20 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #1448: CH2=CHCH2C(O)OCH3 ■ ■ ■ i * ■ • ■ i ■ • ■ ■ i 1 1 I 1 1 1 1 I 43 7.80 8.00 8.20 8.40 m/z 41.05 6.81% 5000

58 T‘01‘0011—00m—310001-0ummn— 72 100 eapmmpmaagmmmg - T m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 7.80 8.00 8.20 8.40

11575.D GCMS0520.M Wed May 22 13:58:48 2002 Page 1

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