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Document / 8 pages

GCMS blank analysis results, May-June 2002

Machine-extracted title · confidence 100%

Laboratory report confirming the absence of target compounds in a procedural blank sample to verify analytical cleanliness.

NYC-WTC_000012653–000012660

Folder label: “GCMS X 5-20-02 A 5-22-02

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Scanned page image, NYC-WTC_000012657
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\MAY2102\LB.D Vial: 3 Acq On : 22 May 2002 3:22 am Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.110 331 335 364 rBV 453521 1113361 36.01% 6.665% 2 12.142 769 775 792 rVB 986015 2370154 76.67% 14.189% 3 15.771 1165 1171 1187 rBV 1555325 3091536 100.00% 18.507% 4 21.077 1744 1750 1761 rBV 1525496 3043358 98.44% 18.219% 5 23.221 1976 1984 1992 rBV 751636 1506679 48.74% 9.020% 6 25.521 2228 2235 2246 rBV2 1218181 2627870 85.00% 15.732% 7 27.500 2445 2451 2458 rBV 39902 77878 2.52% 0.466% 8 33.576 3107 3114 3128 rBV 716811 1616045 52.27% 9.674% 9 37.782 3565 3573 3597 rBV2 432308 1257533 40.68% 7.528%

Sum of corrected areas: 16704414 LB.D GCMS0520.M Wed May 22 13:59:19 2002

NYC-WTC_000012657

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NYC-WTC_000012657Source: NYC Law Department, mirrored locally

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