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GCMS pesticide analysis results, sample AE11573, May-June 2002

Machine-extracted title · confidence 100%

Laboratory report showing analytical results for pesticides and related compounds with values below method reporting limits.

NYC-WTC_000012615–000012649

Folder label: “525 NOT OVR SAMPLE

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 ► Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) 2** Title : Quantitation For Method 525.2 Smoothing : OFF Filtering: 5 *** Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 11.475 41 44 50 rVB2 38190 75183 1.02% 0.152% 2 11.593 50 57 64 rBV 41287 80114 1.08% 0.162% 3 13.108 219 224 229 rBV 2468369 3998371 54.04% 8.102% 4 14.749 402 405 410 rBV 64950 118295 1.60% 0.240% 5 15.566 490 495 499 rVB2 57273 113059 1.53% 0.229%

6 18.187 779 784 789 rBV 4282757 7244845 97.92% 14.680% 7 18.269 789 793 799 rVB2 79859 141637 1.91% 0.287% 8 18.523 817 821 829 rBV2 2486461 4330675 58.53% 8.775% 9 18.967 864 870 873 rVB 68449 118944 1.61% 0.241% 10 19.965 975 980 984 rBV 71165 114038 1.54% 0.231%

11 21.362 1131 1134 1144 rVB 56328 120762 1.63% 0.245% 12 21.951 1193 1199 1203 rBV3 55811 122351 1.65% 0.248% 13 22.514 1253 1261 1267 rBV2 3966718 7398748 100.00% 14.992% 14 22.722 1279 1284 1288 rW2 50345 94191 1.27% 0.191% 15 24.654 1491 1497 1500 rBV2 66926 171385 2.32% 0.347%

16 26.622 1708 1714 1727 rBV2 3096256 5977939 80.80% 12.113% 17 27.393 1793 1799 1811 rBV 3458966 6718312 90.80% 13.614% 18 29.570 2034 2039 2051 rBV 2042881 4134028 55.87% 8.377% 19 30.287 2113 2118 2138 rBV2 2415725 5664486 76.56% 11.478% 20 30.949 2187 2191 2197 rBV2 37935 110041 1.49% 0.223%

21 34.305 2555 2561 2576 rBV 794705 2502725 33.83% 5.071%

Sum of corrected areas: 49350129

1311RR.D 052802.M Mon Jun 03 15:50:11 2002 Page 1

NYC-WTC_000012619

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NYC-WTC_000012619Source: NYC Law Department, mirrored locally

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