GCMS reference analysis report, sample AE04337, March 27, 2002

V M&*s ~~&t Vi RSpOL \NVt ASv.Cwsu) 2 2 K - Data File : C:\MSDCHEM\1\DATA\032602\REF2B326.D Vial: 28 o O 2o Acq On Sample Mise : 27 Mar 2002 : REF 2 : 3/1/02 3:34 am Operator: Inst : McLean Instrumen co — Multiplr: 1.00 "0 I MS Integration Params: BENZO.P C o O o Quant Time: Mar 27 9:03 2002 o Quant Results File: 5080302.RES o' o "0 N o Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) — N Title : Quantitation For Method 508gcscan 0 Last Update : Wed Mar 27 06:57:36 2002 O o Response via : Initial Calibration Q C Abundance TIC: REF2B326.D 3 CD

5500000 1s o d £ o 5000000 § z Is s 45000001 f CM

4000000 L s 2 ©

3500000] l 3000000 I s f 9 8 CI

8 N

I i d

2500000 it ss 8w *3 £ 5 s s I fj 5 S. B9 £ 1 a. st © © 13

i [l 8 © s1 * © a i g§ I ! t > «. f } 2000000 G l ,l i l I ? S § §. 5 I 1 u 5 “ *3 m 5 f is t c 1500000 S ’ t

s I §8 i s f s85 55 St © § a f3 Il IE sS If 1000000 S S 18:7 354 C s I 4 8 3or 2 t * — % 5 53* i JI N

500000 $ 2 1 f x X

Time—> 0-44 TTT 4.00 6.00 TI 8.00 II JU -Pryyt l Ir 10.00 12.00 14.00 16.00 18.00 20.00 22'00 24.00 r* r 1 Pr PT 26.00 28.00 30.00 32.00 T 34.00 r 36.00 38.00 Tni

REF2B326.D 5080302.M Wed Mar 27 09:03:57 2002 Page 3