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GCMS calibration data for sample AE04038, March 2002

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Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.

NYC-WTC_000011711–000011718

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR22O2\REFA2 .D Vial: 18 Acq On : 23 Mar 2002 12:48 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 27 8:48 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.24 168 155963 8.38 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.31 248 110503 10.10 ug/1 89 32) Hexachlorobenzene 24.75 284 125896 9.91 ug/1 # 91 3 3) Phenanthrene 25.72 178 600591 10.09 ug/1 99 34) Anthracene 25.85 178 553869 9.38 ug/1 99 35) Di-n-butylphthalate 27.62 149 759528 10.14 ug/1 98 3 6) Fluoranthene 29.35 202 601687 9.64 ug/1 95 39) Pyrene 30.03 202 619727 12.04 ug/1 94 40) Butylbenzylphthalate 32.15 149 273841 10.32 ug/1 94 41) Benzo(a)anthracene 33.66 228 416046 9.72 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 340218 9.49 ug/1 96 43). Chrysene 33.79 228 446003 10.62 ug/1 98 45) Di-n-Octylphthalate 35.67 149 416493 9.31 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 334591m 10.79 ug/1 47) Benzo(k)fluoranthene 36.84 252 365594 12.09 ug/1 96 48) Benzo(a)pyrene 37.77 252 216690 7.67 ug/1 # 96 49) Indeno(l,2,3-cd)pyrene 42.10 276 232720 6.82 ug/1 96 50) Dibenz(a,h)anthracene 42.18 278 201738 7.64 ug/1 97 51) Benzo (g,h,i)perylene 43.35 276 201087 7.22 ug/1 96

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Wed Mar 27 08:49:30 2002 Page 2

NYC-WTC_000011717

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NYC-WTC_000011717Source: NYC Law Department, mirrored locally

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