GCMS calibration data for Method 508, Mar 11-14 2002

2udtdtct.li CCpIL NUL EtVAEwcu/ 2 2 - Data File : C:\MSDCHEM\l\DATA\031102\CCKA0311.D - O Vial: 10 O 2 Acq On Sample : 11 Mar 2002 : CAL CK STD 7:00 pm Operator: McLean Inst : Instrumen co — o Mise : Multiplr: 1.00 "0 I O O MS Integration Params: BENZO.P C O O O Quant Time: Mar 14 12:32 2002 Quant Results File: 5080302.RES o "0 O. Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) o o — O. Title : Quantitation For Method 508gcscan 0 Last Update : Thu Mar 14 13:02:27 2002 o o Response via : Initial Calibration Q C Abundance TIC: CCKA0311.D 3 CD 7500000 8 d 7000000 £ 5 o2 & 6500000 £ 1 f 8s # It 8 g gt s8 I 8 £ J N w 6000000 : 6

1 © s © 5 a 8 G b 8 5500000 § 78 t J i S.N 8f § 73 I2 t § § • ! 81 £ § 4 5.2 88 8 1B 8 a. 8 g l. 5000000 t F 5 ii < ► if S £ 5 $ , a F u 4500000 s gl 3 © 5 J i I i 4000000 g .8 4 1. 8 > f s I 1 1 D © y 2 8 58 c 8 .2 i § 1I 3500000 z ! o G 8— 5N 5 3 3000000 f 1 5 £ ।i 2500000

2000000 ze I 5

1 4 8

I5 SB

1500000 l 8 5 CD

1000000

500000

0■ • i ■ 1 6.00 1 1 * ‘ r J rr Y ¥ 14.00 Tt — tr f—T 117 " T1 T 28—' I 1 1 11 ■' 1 1 I Time—> 4.00 8.00 10.00 12.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 ‘ i • 32.00 34.00 36.00 38.00 CCKA0311.D 5080302.M Fri Mar 15 15:17:03 2002 Page 3