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GCMS calibration data for Method 508, Mar 29 2002

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for GC/MS analysis using Method 508 conducted on March 29, 2002.

NYC-WTC_000011566–000011574

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• •Data File : C:\MSDCHEM\1\DATA\032202\3437.D Vial: 43 Acg On : 22 Mar 2002 6:34 pm Operator: McLean Sample : 2/14/02 REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.565 418 423 430 rBV 572535 1180164 6.12% 1.177% 2 9.554 1093 1102 1123 rBV 5592884 13673330 70.92% 13.641% 3 13.038 1684 1695 1716 rBV 8743392 18303805 94.94% 18.260% 4 18.156 2554 2566 2580 rBV 8406143 19097332 99.05% 19.052% 5 22.516 3295 3308 3325 rBV2 7538377 19280335 100.00% 19.234%

6 22.651 3327 3331 3343 rVB3 80614 201916 1.05% 0.201% 7 27.433 4138 4145 4159 rBV2 723303 1447962 7.51% 1.445% 8 30.330 4622 4638 4661 rBV2 5926380 16888493 87.59% 16.848% 9 34.202 5281 5297 5319 rBV2 3744316 10165731 52.73% 10.141%

Sum of corrected areas: 100239068

3437.D 5080302.M Mon Mar 25 11:20:11 2002 Page 1

NYC-WTC_000011571

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NYC-WTC_000011571Source: NYC Law Department, mirrored locally

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