GCMS analysis results for sample AE03282, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

'•Data File : C:\MSDCHEM\1\DATA\031902\3282.D Vial: 36 Acq On : 21 Mar 2002 11:07 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 25 09:04:16 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.55 150 3929317 20.00 ug/L 0.00 10) Naphthalene-d8 13.04 136 10214066 20.00 ug/L 0.00 17) Acenaphthene-diO 18.15 164 5654734 20.00 ug/L 0.00 29) Phenanthrene-diO 22.51 188 8760528 20.00 ug/L 0.02 38) Chrysene-dl2 30.33 240 7398980 20.00 ug/L 0.00 44) Perylene-dl2 34.21 264 4126554 20.00 ug/L 0.02

System Monitoring Compounds 0.00 6. 90 37) 2,4-ddd surr 27.44 235 295084 2.82 ug/L Spiked Amount 5.000 Recovery = 56.40%

Target Compounds Qvalue O 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ‘ - oxybis (1-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 2 0) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2 -Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. d 34) Anthracene 0.00 178 0 N.D. d 35) Di-n-butylphthalate 24.65 149 25635 0.06 ug/L 97 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 28.95 149 3271 0.01 ug/L # 16 41) Benzo (a) antracene 30.33 228 18131 0.05 ug/L 63 42) Bis (2-ethylhexyl) phthala 30.91 149 11407 0.04 ug/L 89 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 3282.D 5080302.M Mon Mar 25 09:04:56 2002 Page 1

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