GCMS reference analysis results for sample AE03265, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

• -Data File : C:\MSDCHEM\1\DATA\031902\0214REF2.D Vial: 32 Acq On : 20 Mar 2002 5:53 pm Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise : Multipir: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 25 09:00:05 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1184458 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3111421 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 1711439 20.00 ug/L 0.00 29) Phenanthrene-diO 22.50 188 2653567 20.00 ug/L 0.00 38) Chrysene-dl2 30.31 240 2424363 20.00 ug/L 0.00 44) Perylene-dl2 34.18 264 1316069 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 228245 7.21 ug/L 0.00 Spiked Amount 5.000 Recovery = 144.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.61 74 135633 5.10 ug/L 100 3) bis(2-chloroethyl) ether 8.98 93 440830 10.51 ug/L 84 4) 1,3 - Dichlorobenze 9.38 146 316869 7.64 ug/L 93 5) 1,4 - Dichlorobenzene 9.59 146 334030 8.08 ug/L 98 6) 1,2 - Dichlorobenzene 9.96 146 361727 9.45 ug/L 97 7) 2,2 1 - oxybis (l-Chloropr 10.43 45 1070957 11.21 ug/L 100 8) N-Nitroso-di-n-propylamine 10.75 70 348919 11.57 ug/L 98 9) Hexachloroethane 10.86 117 105568 6.79 ug/L 95 11) Nitrobenzene 11.10 77 433344 7.73 ug/L 99 12) 1sophorone 11.81 82 994894 9.65 ug/L 98 13) bis(2-Chloroethoxy) methan 12.55 93 536522 8.65 ug/L 99 14) 1,2,4-Trichlorobenzene 12.90 180 285840 8.02 ug/L 98 15) Naphthalene 13.08 128 1270861 9.83 ug/L 99 16) Hexachlorobutadiene 13.53 225 112803 5.66 ug/L 98 18) Hexachlorocyclopentadiene 15.60 237 11073 0.73 ug/L 71 19) 2-chloronaphthalene 16.51 162 714059 9.14 ug/L 99 20) Dimethylphthalate 17.59 163 1012165 10.85 ug/L 98 21) 2,6-Dinitrotoluene 17.70 165 179585 9.05 ug/L 95 22) Acenaphthylene 17.69 152 1086366 10.02 ug/L 98 2 3) Acenaphthene 18.22 153 779424 10.58 ug/L 97 24) 2,4-Dinitrotoluene 18.85 165 223294 7.86 ug/L 96 25) Diethylphthalate 19.72 149 944029 11.76 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.89 204 461924 10.80 ug/L 99 27) Fluorene 19.76 166 1005777 11.58 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.34 77 1171744 9.90 ug/L 98 30) N-Nitrosodiphenylamine 20.26 169 424278 7.44 ug/L 96 31) 4-Bromophenyl-phenyl ether 21.32 248 270115 11.53 ug/L 99 32) Hexachlorobenzene 21.34 284 282416 11.43 ug/L 95 3 3) Phenanthrene 22.56 178 1401133 11.40 ug/L 99 34) Anthracene 22.70 178 1269279 10.41 ug/L 99 35) Di-n-butylphthalate 24.64 149 1612093 11.45 ug/L 98 3 6) Fluoranthene 26.06 202 1626939 11.65 ug/L 99 39) Pyrene 26.69 202 1721154 10.27 ug/L 97 40) Butylbenzylphthalate 29.05 149 623249 8.69 ug/L 99 41) Benzo (a) antracene 30.29 228 1292740 10.16 ug/L 98 42) Bis (2-ethylhexyl) phthala 30.91 149 929219 9.80 ug/L 98 43) Chrysene 30.38 228 1437408 11.89 ug/L 99 45) Di-n-Octylphthalate 32.75 149 1270616 8.99 ug/L 99 46) Benzo (b) fluoranthene 33.23 252 1020592 11.00 ug/L 99

(#) = qualifier out of range (m) = manual integration 0214REF2.D 5080302.M Mon Mar 25 09:00:09 2002 Page 1

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