GCMS analysis results for sample AE03076, March 2002

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Laboratory report documenting GC/MS analysis of environmental sample AE03076 conducted on March 22, 2002.

NYC-WTC_000011096–000011104

Folder label: “GCMS X 2/12/02 A 3/19/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

. • Data File : C:\MSDCHEM\1\DATA\031802\3076.D Vial: 7 Acq On : 19 Mar 2002 7:06 am Operator: McLean Sample : GC/MS SCAN 3/6 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 19 21:32:24 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\1\5973N\5080302 .M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.55 150 1345593 > 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 -- 136 3555664 20.00 - ug/L 0.00 17) Acenaphthene-dlO 18.13 164 2019996 20.00 ug/L 0.00 29) Phenanthrene-diO 22.50 188 3152795 20.00 ug/L 0.00 38) Chrysene-dl2 30.30 240 2871084 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1534163 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 268742 7.15 ug/L 0.00 Spiked Amount 5.000 Recovery = 143.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ‘ - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 18.13 165 263903 11.26 ug/L # 25 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 24.65 149 36721 0.22 ug/L 96 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 30.91 149 3817 0.03 ug/L 93 43) Chrysene 30.30 228 8057 0.06 ug/L 57 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 3076.D 5080302.M Tue Mar 19 21:33:18 2002 Page 1

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