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Document / 19 pages

GCMS analysis results for sample AE02720, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02720 including surrogate recovery.

NYC-WTC_000011027–000011045

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) • • Data File : C:\MSDCHEM\l\5973N\02FEB28\02720.D Vial: 5 Acq On : 28 Feb 2002 6:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Mar 01 09:03:00 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1518931 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 6594257 20.00 ug/L 0.00 17) Acenaphthene-diO 18.34 164 3317757 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.63 188 5556003 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 4631181 20.00 ug/L -0.03 44) Perylene-dl2 34.42 264 3264987 20.00 ug/L -0.03

System Monitoring Compounds 37) 2,4-DDD 27.72 235 418136 5.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 113.00% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 535753 2.66 ug/L + 58 21) 2,6-Dinitrotoluene 18.33 165 427566 9.20 ug/L # 27 35) Di-n-butylphthalate 24.86 149 146882 0.41 ug/L 97

/V)

(#) = qualifier out of range (m) = manual integration 02720.D HP022102.M Fri Mar 01 09:03:01 2002 Page 1

NYC-WTC_000011029

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NYC-WTC_000011029Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

9 shared non-person entities · 1 shared topics · similarity 0.998

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