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GCMS results for vial 20, Feb 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing gas chromatography-mass spectrometry analysis of spiked compounds in sample vial 20.

NYC-WTC_000010815–000010822

Folder label: “GCMS X 2/4/02 - 2/28/02

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Scanned page image, NYC-WTC_000010818
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NYC 9/11 Public Portal Document LSC Area Percent Report

’ Data File : C:\MSDCHEM\l\DATA\022702\02577.D Vial: 20 Acq On : 28 Feb 2002 1:29 am Operator: McLean Sample : GC SCAN 2/4 B Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation : 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.865 84 87 94 rBV 92116 202285 1.41% 0.254% 2 9.579 711 717 736 rBV 4253121 9729346 68.00% 12.238% 3 13.062 1094 1101 1105 rBV 6713902 12914816 90.27% 16.244% 4 18.178 1657 1665 1679 rBV 6424267 13912919 97.24% 17.500% 5 22.541 2138 2146 2158 rBV2 6060995 14307515 100.00% 17.996%

6 22.677 2158 2161 2169 rVB2 59445 148442 1.04% 0.187% 7 27.457 2684 2688 2695 rBV 636515 1149144 8.03% 1.445% 8 30.350 2999 3007 3028 rBV 5322063 14268207 99.73% 17.947% 9 30.640 3034 3039 3056 rVB 643855 1385965 9.69% 1.743% 10 34.232 3426 3435 3458 rBV2 4089043 11485299 80.27% 14.446%

Sum of corrected areas: 79503938

32577.D 5080202.M Fri Mar 01 09:03:55 2002 Page 1

NYC-WTC_000010818

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NYC-WTC_000010818Source: NYC Law Department, mirrored locally

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