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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\030402\2338.D Vial: 10 Acq On : 4 Mar 2002 5:38 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last . PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 7.520 482 490 500 rBV2 32256 136745 1.41% 0.215% 2 8.935 641 646 653 rVB 125061 235933 2.43% 0.371% 3 9.579 711 717 736 rBV 2669575 6666696 68.62% 10.477% 4 12.082 988 993 1003 rVB2 726674 1237081 12.73% 1.944% 5 13.053 1094 1100 1114 rBV 4671871 8816297 90.74% 13.855%

6 13.670 1164 1168 1174 rBV2 53201 109811 1.13% 0.173% 7 15.139 1325 1330 1336 rBV 1214514 2041595 21.01% 3.208% 8 15.983 1418 1423 1433 rBV 114207 203824 2.10% 0.320% 9 17.878 1626 1632 1638 rVB 861828 1550071 15.95% 2.436% 10 18.169 1657 1664 1674 rBV 4747262 9564724 98.44% 15.031% 11 18.794 1729 1733 1740 rBV 115090 208422 2.15% 0.328% 12 20.309 1895 1900 1907 rBB 672733 1157151 11.91% 1.818% 13 22.413 2127 2132 2138 rBV 532143 932276 9.60% 1.465% 14 22.522 2138 2144 2157 rW2 4401404 9715865 100.00% 15.269% 15 22.677 2157 2161 2172 rVB2 34192 102451 1.05% 0.161%

16 24.291 2334 2339 2345 rBB 392201 716295 7.37% 1.126% 17 26.005 2522 2528 2534 rBB 318465 626957 6.45% 0.985% 18 27.457 2683 2688 2694 rBV 593972 1040103 10.71% 1.635% 19 27.556 2694 2699 2706 rVB 307120 643139 6.62% 1.011% 20 28.989 2851 2857 2868 rBV 263432 580428 5.97% 0.912% 21 30.341 2998 3006 3027 rBV2 4055963 9681175 99.64% 15.214% 22 31.620 3141 3147 3159 rBV 174932 473087 4.87% 0.743% 23 32.817 3273 3279 3292 rBV2 122026 344694 3.55% 0.542% 24 33.933 3397 3402 3414 rBV 85961 240803 2.48% 0.378% 25 34.214 3425 3433 3448 rBV 2692794 6334277 65.20% 9.954% 26 34.985 3513 3518 3526 rBV2 57676 158094 1.63% 0.248% 27 36.001 3621 3630 3636 rBV2 42103 114918 1.18% 0.181%

Sum of corrected areas: 63632912

2338.D 5080302.M Mon Mar 18 08:32:06 2002 Page 1

NYC-WTC_0000 10590

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NYC-WTC_000010590Source: NYC Law Department, mirrored locally

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