GCMS Method 508 log data, Jan-Mar 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C: \MSDCHEM\1\DATA\0304 02\DFTPP. D Vial: 1 Acq On 4 Mar 2002 6:00 am Operator: McLean Sample DFTPP Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan

Abundance TIC: DFTPP.D 6000000

5000000

4000000

3000000

2000000

1000000

0- ■ ■ i ■ • ■ 1 i ' ' ■ ■ i ■ • ■ • i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ ■ i • ■ ‘ ■ i ■ ‘ ‘ • I ■ TIan0)uuubuunePmTuit lime—> 22.00 22.20 22.40 22.60 22.80 23.00 23.20 23.40 23.60 23.80 24.00 24.20 24.40 24.60 24.80 25.00 25.20 25.40 25.60 Abundance Average of 23.820 to 23.883 min.: DFTPP.D 198

250000 442

200000 51 150000 77 255 127

100000 110 275 50000 224

m/z-> 0 — 464 1 + 44 1 4 I, H+H# 4 H | (11 TT 4.242.1 +4210323 352305,,383 403. 23. Irr 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 23.820 to 23.883 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 10 80 57.8 161267 PASS 68 69 0.00 2 1.4 1831 PASS 69 198 0.00 100 46.4 129443 PASS 70 69 0.00 2 0.4 520 PASS 127 198 10 80 48.9 136448 PASS 197 198 0.00 2 0.2 557 PASS 198 198 50 100 100.0 279083 PASS 199 198 5 9 6.6 18447 PASS 275 198 10 60 22.0 61482 PASS 365 198 1 100 2.6 7309 PASS 441 443 0.01 100 77.8 34826 PASS 442 198 50 100 83.4 232814 PASS 443 442 15 24 19.2 44746 PASS

DFTPP.D 5080302.M Mon Mar 18 06:59:03 2002

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