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GCMS analysis results for sample AE01687, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01687 conducted on March 4, 2002, including surrogate recovery data.

NYC-WTC_000010196–000010204

Folder label: “GCMS X 1/25/02 A 2/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C: \HPCHEM\1\DATA\FEB2502\1687.D Vial: 8 Acq On : 25 Feb 2002 6:24 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.195 339 343 348 rBV 8801 19431 1.04% 0.224% 2 12.317 787 792 806 rVB 537377 1366253 72.82% 15.772% 3 15.952 1182 1188 1200 rBV 830586 1765397 94.09% 20.380% 4 21.268 1761 1767 1780 rBV 903173 1876270 100.00% 21.660% 5 25.711 2245 2251 2263 rBV2 753696 1633811 87.08% 18.861%

6 30.788 2800 2804 2811 rBV 88464 168188 8.96% 1.942% 7 33.780 3123 3130 3145 rBV2 432090 1042893 55.58% 12.039% 8 38.049 3587 3595 3609 rBV2 254780 790080 42.11% 9.121%

Sum of corrected areas: 8662323

1687.D GCMS0208.M Thu Feb 28 09:31:16 2002

NYC-WTC_000010201

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NYC-WTC_000010201Source: NYC Law Department, mirrored locally

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