GCMS analysis results for sample AE01638, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. . Data File : C:\MSDCHEM\l\5973N\02FEB21\01638 .D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Pentanone, 1-phenyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

19.99 0.05 ug/L 37111 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 1-phenyl- 162 C11H14O 006683-92-7 4 2 1-PHENYLPENTAN-2-ONE $$ 2-Pentan... 162 C11H14O 006683-92-7 4 3 1-PHENYLPENTAN-2-ONE $$ 2-Pentan... 162 C11H140 006683-92-7 4 4 l-Methoxy-4-phenyl-1-butene 162 C11H14O 000000-00-0 4 Abundance Scan 1472 (19.991 min): 01638.D (-) m/z 71.00 100.00% 71

5000 149 43 84 162 ...... N,...... . 19.60 19.80 20.00 20.20 20.40

n/z-> 01 ... 1 . 804 20 30 90 100 110 120 130 140 150 160 170 40 50 60 70 TTTT m/z 149.00 39.30% Abundance #62391:2-Pentanone, 1-phenyl- 4 71 91

5000 19.60 19.80 20.00 20.20 2040 27 162 m/z43.10 26.86% 63 128 0------ 11-00110902000003’ TTTIr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #62393:1-PHENYLPENTAN-2-ONE $$ 2-Pentanone, 1-phenyl- (CA... 71 19.60 19.80 20.00 20.20 20.40 91 5000 m/z 162.10 18.26% 27 51 105 162 78 119 0 ■ I ■ ■1 ■ i'' ■ ■ i ■ ■ ' ■ 1 ■ ■ ■ ''I1 TIWWIWPPnuui ■11 ■11' I 111 ■ ■ III" miz-> 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 Abundance #62397:1-PHENYLPENTAN-2-ONE $$ 2-Pentanone, 1-phenyl- (CA... It ■ ■ i ■ • • i • 71 19.60 19.80 20.00 20.20 20.40 m/z 41.10 14.49%

5000 91

162

0- ■ i “ 1 • i ■ ■ ■ ■ i ■ “ ‘ i • ■ ■ ■ i ■ ■1 ■ i “ • ■ i • ■ ■ ■ i1' •' i ■ ■ ■11 ■ “ ■ i1 ■'' i ■ ■ ‘111" ‘ i ■ ■ " i 1 ■ i ■ ‘ i ■ ■ ■ ■ i ' ■ -r-r-p-r-T-r-j-n m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 19.60 19.80 20.00 20.20 20.40

01638.D HP022102.M Mon Feb 25 10:55:51 2002 Page 10

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