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GCMS analysis report for sample AE01636, March 2002

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GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010086–000010105

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report ■ Data File : C: \MSDCHEM\1\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

3.62 0.17 ug/L 72502 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 Abundance Scan 22 (3.622 min): 01636.D (-) m/z 43.10 100.00% 43 74 |........ f 5000 59 87 1' i ■1 3.50 3.60 3.70 3.80 3.90 4.00

iz-> 0! 1—44488011184-184*41 +51i1 ■" i ■"' i 11’17111 “ i' “ ■ i ■1 ■11 “ •' i • ■ • ■ i ‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/z 74.00 95.92% Abundance #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74

5000 ‘ 3.50 3.60 3.70 3.80 3.90 4.00 ‘ ‘ ‘ 59 87 m/z 71.00 66.12% 33 102 01 • ■ l * ‘ • i"1 * 11' ’ ‘ l ’1 ‘ ‘ 11 +t * J'" • 11 1' i"'' I'' "I11" I' ■ ■' 11 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #9228: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 .. ।.,.. ।.. A ।.... 111111 Ci 1111111 3.50 3.60 3.70 3.80 3.90 4.00 5000 m/z 59.00 29.43% 59 87

102 0 ' I'''' I''' ‘ I' I +t tpmp t,| j.. I ! | ' I I ' | I I I I ] 1 _........................ mfz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #9224: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... ■ 11 ‘ ‘ 4)3 3.50 3.60 3.70 3.80 3.90 4.00 74 m/z 41.10 28.90% 5000- 27 59 87 33 69 102 0 ■■-I1'1'! '■ "I ■ T-p-n-rp-rr mT +t pmp mmnp—uBunr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 66 3.60 3.70 3.80 566 4.00

01636.D HP022102.M Mon Feb 25 10:55:37 2002 Page 3

NYC-WTC_000010092

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NYC-WTC_000010092Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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