GCMS calibration results, Feb 20, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB110 2\CAL8 0A.D Vial: 2 Acq On 12 Feb 2002 3:22 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 15:26 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.36 152 307062 20.00 ug/1 0.00 10) Naphthalene-d8 16.01 136 1170599 20.00 ug/1 0.00 17) Acenaphthene-diO 21.32 164 677285 20.00 ug/1 0.00 29) Phenanthrene-diO 25.77 188 950753 20.00 ug/1 0.00 38) Chrysene-dl2 33.85 240 749078 20.00 ug/1 0.00 44) Perylene-dl2 38.14 264 454911 20.00 ug/1 0.02

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 6.00 74 993060 80.82 ug/1 95 3) bis(2-Chloroethyl)ether 11.77 93 1740701 86.25 ug/1 99 4) 1,3-Dichlorobenzene 12.26 146 1986271 82.69 ug/1 100 5) 1,4-Dichlorobenzene 12.41 146 2068056 84.47 ug/1 98 6) 1,2-Dichlorobenzene 12.93 146 1976644 84.97 ug/1 100 7) 2,2'-oxybi s(1-Chioropropan 13.24 45 2648640 86.69 ug/1 98 8) N-Nitroso-di-n-propylamine 13.67 70 1234757 85.52 ug/1 95 9) Hexachloroethane 13.77 117 813556 83.01 ug/1 95 11) Nitrobenzene 14.07 77 1959543 81.41 ug/1 99 12) 1sophorone 14.73 82 3506882 86.24 ug/1 99 13) bis(2-Chloroethoxy)methane 15.40 93 2200555 86.89 ug/1 99 14) 1,2,4-Trichlorobenzene 15.90 180 1713553 85.53 ug/1 98 15) Naphthalene 16.08 128 5408409 86.75 ug/1 100 16) Hexachlorobutadiene 16.60 225 1003074 83.67 ug/1 99 18) Hexachlorocyclopentadiene 18.80 237 792065 81.69 ug/1 99 19) 2-Chloronaphthalene 19.59 162 3334112 82.57 ug/1 99 20) Dimethylphthalate 20.69 163 3833473 81.52 ug/1 100 21) 2,6-Dinitrotoluene 20.91 165 882984 82.84 ug/1 96 22) Acenaphthylene 20.86 152 4877571 83.61 ug/1 100 2 3) Acenaphthene 21.43 153 3392243 83.20 ug/1 100 24) 2,4-Dinitrotoluene 22.09 165 1117677 82.77 ug/1 91 25) Diethylphthalate 22.84 149 4029417 82.44 ug/1 98 26) 4-Chlorophenyl-phenylether 22.96 204 1695417 80.58 ug/1 100 27) Fluorene 22.96 166 3691586 82.96 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.45 77 4301361 83.67 ug/L 91

(#) = qualifier out of range (m) = manual integration CAL80A.D GCMS0208.M Tue Feb 19 15:27:33 2002 Page 1

NYC-WTC_000009438