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GCMS Method 508 data table, Feb 2002

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Laboratory data table recording drip rates and volumes for GCMS Method 508 analysis.

NYC-WTC_000009428–000009436

Folder label: “GCMS X 1/14/02 A 2/25-2/26

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1102\LBB.D Vial: 30 Acq On : 12 Feb 2002 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 12 17:10 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.76 178 181 N.D. 34) Anthracene 25.76 178 181 N.D. 35) Di-n-butylphthalate 27.72 149 2312 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 30.13 202 229 N.D. 40) Butylbenzylphthalate 32.25 149 600 N.D. 41) Benzo(a)anthracene 33.89 228 4615 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 2460 N.D. 43) Chrysene 33.89 228 4448 N.D. 45) Di-n-Octylphthalate 35.77 149 1332 N.D. 4 6) Benzo(b)fluoranthene 36.90 252 2026 N.D. 47) Benzo(k)fluoranthene 36.97 252 2928 N.D. 48) Benzo(a)pyrene 37.90 252 1183 N.D. 4 9) Indeno(1,2,3-cd)pyrene 42.35 276 218 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.63 276 837 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D GCMS0208.M Tue Feb 19 15:28:53 2002 Page 2

NYC-WTC_000009430

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NYC-WTC_000009430Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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